Pentamethylcyclopentadienyltitanium trichloride synthesis
- Product Name:Pentamethylcyclopentadienyltitanium trichloride
- CAS Number:12129-06-5
- Molecular formula:C10H15Cl3Ti
- Molecular Weight:289.45
136990-69-7
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75-77-4
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12129-06-5
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Yield:12129-06-5 99%
Reaction Conditions:
in toluene;Dropwise addn. of TiCl4 in toluene to soln. of C(CH3)5Si(CH3)3 in toluene (N2), stirring (2 h, color change from red-orange to red).; Evapn. of solvent and byproduct (vacuum), washing of crystals (pentane), dried (vacuum), elem. anal.;
References:
Llinas, Gerardo Hidalgo;Mena, Miguel;Palacios, Federico;Royo, Pascual;Serrano, Ricardo [Journal of Organometallic Chemistry,1988,vol. 340,p. 37 - 40]
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11136-36-0
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4045-44-7
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7550-45-0
313 suppliers
$10.00/10g
12129-06-5
110 suppliers
$30.00/250mg