Phenanthrene, 3-chloro-9-phenyl- synthesis

7synthesis methods

Product Name:Phenanthrene, 3-chloro-9-phenyl-
CAS Number:94546-54-0
Molecular formula:C20H13Cl
Molecular Weight:288.77

106-39-8 Synthesis

106-39-8
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24892-82-8
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94546-54-0
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Yield:94546-54-0 61%

Reaction Conditions:

with palladium diacetate;potassium carbonate;bis[2-(diphenylphosphino)phenyl] ether in 1,4-dioxane at 130; for 5 h;Inert atmosphere;Schlenk technique;Sealed tube;regioselective reaction;

References:

Wei, Dong;Li, Meng-Yao;Zhu, Bin-Bin;Yang, Xiao-Di;Zhang, Fang;Feng, Chen-Guo;Lin, Guo-Qiang [Angewandte Chemie - International Edition,2019,vol. 58,# 46,p. 16543 - 16547][Angew. Chem.,2019,vol. 131,# 46,p. 16695 - 16699,5] Location in patent:supporting information

73006-78-7 Synthesis