![](/CAS/GIF/215527-70-1.gif)
PHENYL-D5-BORONIC ACID synthesis
- Product Name:PHENYL-D5-BORONIC ACID
- CAS Number:215527-70-1
- Molecular formula:C6H7BO2
- Molecular Weight:121.93
![Bromobenzene-d5](/CAS/GIF/4165-57-5.gif)
4165-57-5
160 suppliers
$56.29/2g
![PHENYL-D5-BORONIC ACID](/CAS/GIF/215527-70-1.gif)
215527-70-1
155 suppliers
$85.00/250mg
Yield:215527-70-1 98%
Reaction Conditions:
Stage #1:bromobenzene-d5 with n-butyllithium;triethyl borate in tetrahydrofuran at -78 - 20; for 4 h;
Stage #2: with hydrogenchloride;water in tetrahydrofuran at 0 - 20; for 1 h;
Steps:
1.3
(3) Preparation of N,N-di-naphtalen-l-yl-teφhenyl-4,4'-diamine-dl2 [63]1 n-BuLιPd2(dba)3 (0 03 eq)[64] 10 g (61.7 mmol) of bromobenzene-d5 was dissolved in 300 mL of tetrahydrofuran, and then the temperature of the reaction solution was maintained at -78°C. 57.8 mL (92.6 mmol) of 1.6M n-BuLi was then slowly added thereto, and the resulting solution EPO
References:
DOOSAN CORPORATION WO2006/121237, 2006, A1 Location in patent:Page/Page column 7-8
![Triethyl borate](/CAS/GIF/150-46-9.gif)
150-46-9
186 suppliers
$12.00/25mL
![Bromobenzene-d5](/CAS/GIF/4165-57-5.gif)
4165-57-5
160 suppliers
$56.29/2g
![PHENYL-D5-BORONIC ACID](/CAS/GIF/215527-70-1.gif)
215527-70-1
155 suppliers
$85.00/250mg
![Triisopropyl borate](/CAS/GIF/5419-55-6.gif)
5419-55-6
370 suppliers
$12.00/5g
![Bromobenzene-d5](/CAS/GIF/4165-57-5.gif)
4165-57-5
160 suppliers
$56.29/2g
![PHENYL-D5-BORONIC ACID](/CAS/GIF/215527-70-1.gif)
215527-70-1
155 suppliers
$85.00/250mg
![Trimethyl borate](/CAS/GIF/121-43-7.gif)
121-43-7
345 suppliers
$13.00/25mL
![Bromobenzene-d5](/CAS/GIF/4165-57-5.gif)
4165-57-5
160 suppliers
$56.29/2g
![PHENYL-D5-BORONIC ACID](/CAS/GIF/215527-70-1.gif)
215527-70-1
155 suppliers
$85.00/250mg
![Triisopropyl borate](/CAS/GIF/5419-55-6.gif)
5419-55-6
370 suppliers
$12.00/5g
![Bromobenzene-d5](/CAS/GIF/4165-57-5.gif)
4165-57-5
160 suppliers
$56.29/2g
![Water](/CAS/GIF/7732-18-5.gif)
7732-18-5
461 suppliers
$12.69/100ml
![PHENYL-D5-BORONIC ACID](/CAS/GIF/215527-70-1.gif)
215527-70-1
155 suppliers
$85.00/250mg