Propanoic acid, 2-methyl-2-(methylthio)- synthesis
- Product Name:Propanoic acid, 2-methyl-2-(methylthio)-
- CAS Number:27868-56-0
- Molecular formula:C5H10O2S
- Molecular Weight:134.2
Yield:27868-56-0 94%
Reaction Conditions:
Stage #1: ethyl 2-bromoisobutyrate;sodium thiomethoxide in ethanol at 20; for 12 h;
Stage #2: with lithium hydroxide monohydrate in tetrahydrofuran;ethanol;water at 90; for 4 h;
References:
Wang, Rui;Ding, Yongzheng;Li, Gang [Organic and Biomolecular Chemistry,2017,vol. 15,# 23,p. 4966 - 4970] Location in patent:supporting information
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