Propanoic acid, 2-methyl-2-(methylthio)- synthesis

4synthesis methods

Product Name:Propanoic acid, 2-methyl-2-(methylthio)-
CAS Number:27868-56-0
Molecular formula:C5H10O2S
Molecular Weight:134.2

600-00-0 Synthesis

600-00-0
267 suppliers
$13.00/5g

5188-07-8
272 suppliers
$13.00/5g

Propanoic acid, 2-methyl-2-(methylthio)-

27868-56-0
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Yield:27868-56-0 94%

Reaction Conditions:

Stage #1: ethyl 2-bromoisobutyrate;sodium thiomethoxide in ethanol at 20; for 12 h;
Stage #2: with lithium hydroxide monohydrate in tetrahydrofuran;ethanol;water at 90; for 4 h;

References:

Wang, Rui;Ding, Yongzheng;Li, Gang [Organic and Biomolecular Chemistry,2017,vol. 15,# 23,p. 4966 - 4970] Location in patent:supporting information

29786-93-4 Synthesis

29786-93-4
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624-92-0 Synthesis

624-92-0
323 suppliers
$26.39/5ml

547-63-7 Synthesis

547-63-7
226 suppliers
$13.00/5g

27868-56-0
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References

Propanoic acid, 2-methyl-2-(methylthio)-, methyl ester

87122-80-3
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27868-56-0
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References

77-78-1
301 suppliers
$22.00/25g

4695-31-2
63 suppliers
$155.00/500mg

27868-56-0
4 suppliers
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References