ChemicalBook CAS DataBase List PROPARGYL BENZOATE 98

PROPARGYL BENZOATE 98 synthesis

14synthesis methods

Product Name:PROPARGYL BENZOATE 98
CAS Number:6750-04-5
Molecular formula:C10H8O2
Molecular Weight:160.17

107-19-7
5 suppliers
$12.00/25g

65-85-0 Synthesis

65-85-0
1343 suppliers
$10.00/25 g

6750-04-5
30 suppliers
$14.00/250mg

Yield: 97%

Reaction Conditions:

with graphene oxide in 1,2-dichloro-ethane at 100; for 24 h;

Steps:

General procedure for the synthesis of esters from acids and alcohols
General procedure: A mixture of acid (0.2 mmol), alcohol (0.6 mmol) and GO (50 wt%, calculated with the mass of acid) in ethyl alcohol or DCE (1 mL) was placed in a test tube equipped with a magnetic stirring bar. The mixture was stirred at 100 °C for 24 h. After the reaction was finished, filtered the GO, solvent was removed, and the residue was separated by column chromatography to give the pure sample.

References:

Chen, Zhengwang;Wen, Yuelu;Fu, Yejuan;Chen, Hai;Ye, Min;Luo, Guotian [Synlett,2017,vol. 28,# 8,art. no. ST-2016-W0670-L,p. 981 - 985] Location in patent:supporting information

98-88-4 Synthesis