ChemicalBook CAS DataBase List PSI7409

PSI7409 synthesis

7synthesis methods

Product Name:PSI7409
CAS Number:1015073-42-3
Molecular formula:C10H16FN2O14P3
Molecular Weight:500.16

58-96-8 Synthesis

58-96-8
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1015073-42-3
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Yield:-

Steps:

Multi-step reaction with 9 steps
1.1: pyridine / 16 h / Inert atmosphere
2.1: Dess-Martin periodane / dichloromethane / 16 h / 20 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran
4.1: triethylamine hydrofluoride / tetrahydrofuran
5.1: pyridine
6.1: diethylamino-sulfur trifluoride / dichloromethane
7.1: ammonia / methanol
8.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; trimethyl phosphite / tetrahydrofuran / 0.17 h / 20 °C / Sonication; Inert atmosphere
8.2: 1 h / 20 °C / Inert atmosphere
9.1: bis(tri-n-butylammonium) pyrophosphate; tributyl-amine / N,N-dimethyl-formamide / 0.08 h / 20 °C

References:

Wang, Gang;Lim, Siew Pheng;Chen, Yen-Liang;Hunziker, Jürg;Rao, Ranga;Gu, Feng;Seh, Cheah Chen;Ghafar, Nahdiyah Abdul;Xu, Haoying;Chan, Katherine;Lin, Xiaodong;Saunders, Oliver L.;Fenaux, Martijn;Zhong, Weidong;Shi, Pei-Yong;Yokokawa, Fumiaki [Bioorganic and Medicinal Chemistry Letters,2018,vol. 28,# 13,p. 2324 - 2327]

1015073-43-4
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1015073-42-3
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References

863329-66-2 Synthesis

863329-66-2
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1015073-42-3
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References

2,4(1H,3H)-Pyrimidinedione, 1-[2-C-methyl-3,5-O-[1,1,3,3-tetrakis(1-methylethyl)-1,3-disiloxanediyl]-β-D-arabinofuranosyl]-

114262-45-2
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1015073-42-3
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References

1-((2R,3S,4R,5R)-3,4-dihydroxy-5-(hydroxyMethyl)-3-Methyltetrahydrofuran-2-yl)pyriMidine-2,4(1H,3H)-dione

114262-49-6
30 suppliers
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1015073-42-3
37 suppliers
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References