Rhodomyrtone synthesis

6synthesis methods

Product Name:Rhodomyrtone
CAS Number:468757-69-9
Molecular formula:C26H34O6
Molecular Weight:442.54

1H-Xanthene-1,3(2H)-dione, 4,9-dihydro-6,8-dihydroxy-2,2,4,4-tetramethyl-9-(2-methylpropyl)-

1453207-09-4
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108-12-3 Synthesis

108-12-3
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468757-69-9
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Yield:468757-69-9 75%

Reaction Conditions:

Stage #1: 6,8-dihydroxy-9-isobutyl-2,2,4,4-tetramethyl-4,9-dihydro-1H-xanthene-1,3(2H)-dionewith titanium(IV) tetrachloride in dichloromethane;toluene at 20; for 0.25 h;
Stage #2: 3-methylbutanoyl chloride in dichloromethane;toluene at 20 - 80; for 2.16667 h;

References:

Deng, Lu-Ming;Tang, Wei;Wang, Shu-Qin;Song, Jian-Guo;Huang, Xiao-Jun;Zhu, Hao-Yue;Li, Yao-Lan;Ye, Wen-Cai;Hu, Li-Jun;Wang, Ying [Journal of Organic Chemistry,2022,vol. 87,# 7,p. 4788 - 4800]

4-Cyclohexene-1,3-dione, 4-acetyl-5-hydroxy-2,2,6,6-tetramethyl-

7073-22-5
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468757-69-9
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4-Cyclohexene-1,3-dione, 5-hydroxy-2,2,6,6-tetramethyl-

77744-52-6
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468757-69-9
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590-86-3 Synthesis

590-86-3
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468757-69-9
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References

567-75-9
16 suppliers
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468757-69-9
13 suppliers
$291.00/1mg

References