(S)-1-(2-Aminoacetyl)-pyrrolidine-2-carbonitrile synthesis
- Product Name:(S)-1-(2-Aminoacetyl)-pyrrolidine-2-carbonitrile
- CAS Number:914070-99-8
- Molecular formula:C7H11N3O
- Molecular Weight:153.18
214398-99-9
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Yield:-
Reaction Conditions:
Stage #1: (S)-1-(2-chloroacetyl) pyrrolidine-2-carboxamidewith trifluoroacetic anhydride in tetrahydrofuran at 0 - 20; for 6 h;
Stage #2: with ammonium hydroxide at -20 - 20; for 3 h;
References:
Lizza, Joseph R.;Patel, Savan V.;Yang, Catherine F.;Moura-Letts, Gustavo [European Journal of Organic Chemistry,2016,vol. 2016,# 30,p. 5160 - 5168] Location in patent:supporting information
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![L-Prolinamide, N-[(1,1-dimethylethoxy)carbonyl]glycyl-](/CAS/20210111/GIF/52293-28-4.gif)
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