![](/CAS/GIF/79-36-7.gif)
Dichloroacetyl chloride synthesis
- Product Name:Dichloroacetyl chloride
- CAS Number:79-36-7
- Molecular formula:C2HCl3O
- Molecular Weight:147.39
![Trichloroethylene](/CAS/GIF/79-01-6.gif)
79-01-6
438 suppliers
$19.21/100ml
![Dichloroacetyl chloride](/CAS/GIF/79-36-7.gif)
79-36-7
284 suppliers
$15.00/10g
Yield:79-36-7 90%
Reaction Conditions:
with tributyl borane;oxygen at 80; under 2280.15 Torr; for 11 h;Reagent/catalyst;
Steps:
1.1; 2.1; 3.1
Add 1314g (10mol) of trichloroethylene and 18.2g (0.1mol) of tributylboron into the pressure-resistant reactor, then pass in dry oxygen, adjust the pressure of the oxygen to 3 atmospheres, and then increase the temperature React at 80°C for 11h. After the completion of the reaction, atmospheric distillation is performed, and the fractions are collected at a temperature range of 105°C to 108°C to obtain 1,325 g of a colorless and transparent liquid product, dichloroacetyl chloride, with a yield of 90%.
References:
CN111995516,2020,A Location in patent:Paragraph 0041; 0043-0044; 0058; 0060-0061; 0066; 0068-0069
![Dichloroacetic acid](/CAS/GIF/79-43-6.gif)
79-43-6
292 suppliers
$22.00/25g
![Dichloroacetyl chloride](/CAS/GIF/79-36-7.gif)
79-36-7
284 suppliers
$15.00/10g
![Acetyl chloride](/CAS/GIF/75-36-5.gif)
75-36-5
563 suppliers
$17.92/100G
![Dichloroacetyl chloride](/CAS/GIF/79-36-7.gif)
79-36-7
284 suppliers
$15.00/10g
![Chloroacetyl chloride](/CAS/GIF/79-04-9.gif)
79-04-9
354 suppliers
$12.00/5g
![Trichloroacetyl chloride](/CAS/GIF/76-02-8.gif)
76-02-8
251 suppliers
$38.29/25G
![Trichloroacetyl chloride](/CAS/GIF/76-02-8.gif)
76-02-8
251 suppliers
$38.29/25G
![Dichloroacetyl chloride](/CAS/GIF/79-36-7.gif)
79-36-7
284 suppliers
$15.00/10g
![1,1,2,2-Tetrachloroethane](/CAS/GIF/79-34-5.gif)
79-34-5
245 suppliers
$10.00/5g
![Dichloroacetyl chloride](/CAS/GIF/79-36-7.gif)
79-36-7
284 suppliers
$15.00/10g
![Chloroform](/CAS/GIF/67-66-3.gif)
67-66-3
6 suppliers
$33.60/500ml
![PENTACHLOROETHANE](/CAS/GIF/76-01-7.gif)
76-01-7
56 suppliers
$57.20/5ml