ChemicalBook CAS DataBase List S-(4-NITROBENZYL)-6-THIOINOSINE

S-(4-NITROBENZYL)-6-THIOINOSINE synthesis

5synthesis methods

Product Name:S-(4-NITROBENZYL)-6-THIOINOSINE
CAS Number:38048-32-7
Molecular formula:C17H17N5O6S
Molecular Weight:419.41

1-O-ACETYL-2,3,5-TRI-O-BENZOYL-D-RIBOFURANOSE

14215-97-5
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$11.00/5g

38048-32-7
102 suppliers
$45.00/25mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 94 percent / hexamethyldisilazane; Me₃SiCl; trimethylsilyl triflate / acetonitrile / 2.5 h / Heating
2.1: 36 percent / NH₃ / methanol / 20 °C
3.1: trityl resin; pyridine / 48 h
3.2: Et₃N / methanol / 5 h / 55 °C
3.3: 94 percent / triisopropylsilane; trifluoroacetic acid / CH₂Cl₂ / 0.17 h

References:

Yadav, Vikas;Chu, Chung K.;Rais, Reem H.;Al Safarjalani, Omar N.;Guarcello, Vincenzo;Naguib, Fardos N. M.;El Kouni, Mahmoud H. [Journal of Medicinal Chemistry,2004,vol. 47,# 8,p. 1987 - 1996]

26798-33-4 Synthesis