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ChemicalBook CAS DataBase List SCH 58261
160098-96-4

SCH 58261 synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 2-methoxy-ethanol / Heating
2: diphenyl ether / 1.5 h / 260 °C
3: 75 percent / 10percent aq. HCl / 3 h / Heating
4: 20 percent / p-tolenesulfonic acid, N-methylpyrrolidone / 160 °C

References:

Baraldi, Pier Giovanni;Cacciari, Barbara;Spalluto, Giampiero;Pineda De Las Infantas Y Villatoro, Maria José;Zocchi, Cristina;Dionisotti, Silvio;Ongini, Ennio [Journal of Medicinal Chemistry,1996,vol. 39,# 5,p. 1164 - 1171]

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