![](/CAS/GIF/2156-56-1.gif)
Sodium dichloroacetate synthesis
- Product Name:Sodium dichloroacetate
- CAS Number:2156-56-1
- Molecular formula:C2H3Cl2NaO2
- Molecular Weight:152.93
![Dichloroacetic acid](/CAS/GIF/79-43-6.gif)
79-43-6
290 suppliers
$21.00/25g
![Sodium dichloroacetate](/CAS/GIF/2156-56-1.gif)
2156-56-1
292 suppliers
$6.00/1g
Yield:2156-56-1 96%
Reaction Conditions:
with sodium hydroxide in water at 20; for 2 h;
Steps:
Sodium dichloroacetate, Na[Cl2CHCO2] (Chart S5).
A solution of Cl2CHCO2H (135 μL, 1.64 mmol) in H2O (2 mL) was treated with 1.00 M NaOH(1.60 mL, 1.60 mmol) and stirred at room temperature for 2 hours. Volatiles were then removedunder vacuum and the yellowish residue was suspended in acetone. The suspension was filtered andthe resulting colorless solid was washed with acetone and dried under vacuum. Yield: 227 mg, 96%.
References:
Biancalana, Lorenzo;Pampaloni, Guido;Zacchini, Stefano;Marchetti, Fabio [Journal of Organometallic Chemistry,2018,vol. 869,p. 201 - 211] Location in patent:supporting information