Sodium phenoxyacetate synthesis
- Product Name:Sodium phenoxyacetate
- CAS Number:3598-16-1
- Molecular formula:C8H7NaO3
- Molecular Weight:174.13
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Yield:-
Reaction Conditions:
with sodium hydroxide in water; for 8 h;Reflux;
Steps:
2.1 Synthesis of phenoxyacetic acid and ring-substituted phenoxyacetic acids
General procedure: General procedure: To a solution of phenol or ring-substituted phenol (20 mmol) in water (20 mL) was added sodium chloroacetate (22 mmol) at rt. The mixture was heated and stirred at reflux for 8 h. The reaction mixture was cooled and the pH was adjusted to a value of 1.0 with 5 N HCl. The solution was filtered and the obtained solid was recrystallized from dehydrated ethanol to afford the pure product.
References:
He, Xingrui;Yu, Zhaonan;Jiang, Shaojie;Zhang, Peizhi;Shang, Zhicai;Lou, Yonggen;Wu, Jun [Bioorganic and Medicinal Chemistry Letters,2015,vol. 25,# 23,p. 5601 - 5603] Location in patent:supporting information
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