SPhos Pd G1, Methyl t-Butyl Ether Adduct synthesis
- Product Name:SPhos Pd G1, Methyl t-Butyl Ether Adduct
- CAS Number:1028206-58-7
- Molecular formula:C34H45ClNO2PPd
- Molecular Weight:672.58
657408-07-6
339 suppliers
$6.00/1g
13078-80-3
192 suppliers
$10.00/1g
14267-08-4
104 suppliers
$35.00/100mg
917-54-4
172 suppliers
$52.10/25ml
1028206-58-7
90 suppliers
$15.00/100mg
Yield:1028206-58-7 85%
Reaction Conditions:
in further solvent(s);treatment of palladium compd. with methyllithium in methyl tert-butyl ether at 0°C, treatment with chlorobenzene deriv. and phosphine deriv. in methyl tert-butyl ether at 55°C; recrystn.;
References:
Biscoe, Mark R.;Fors, Brett P.;Buchwald, Stephen L. [Journal of the American Chemical Society,2008,vol. 130,# 21,p. 6686 - 6687]