![](/CAS/GIF/2153-28-8.gif)
TERPINYL BUTYRATE synthesis
- Product Name:TERPINYL BUTYRATE
- CAS Number:2153-28-8
- Molecular formula:C14H24O2
- Molecular Weight:224.34
![Butyric anhydride](/CAS/GIF/106-31-0.gif)
106-31-0
214 suppliers
$10.00/5g
![alpha-Terpineol](/CAS/GIF/98-55-5.gif)
98-55-5
366 suppliers
$21.00/25mL
![TERPINYL BUTYRATE](/CAS/GIF/2153-28-8.gif)
2153-28-8
32 suppliers
$259.75/2.5KG
Yield:2153-28-8 80.5%
Reaction Conditions:
with p-toluenesulfonyl chloride at 20; for 1.5 h;
Steps:
4.1.1 General procedure for the synthesis of compounds 2a-f
General procedure: A mixture ofα-terpineol (1, 2mmol), acid anhydride (3mL) and TsCl (0.2mmol) was stirred at room temperaturefor 1.5h, and then neutralized to pH7-8 with 10% NaOH aqueous solution, washed with water (2×10mL) and brine (10mL). The organic layer was separated and dried over anhydrous Na2SO4, then concentrated and purified by silica gel column chromatography (petroleum ether/ethyl acetate=1:5 v/v) to afford the desired products.
References:
Zhu, Wanping;Liu, Xia;Wang, Yuji;Tong, Yeling;Hu, Yongzhou [European Journal of Medicinal Chemistry,2018,vol. 143,p. 419 - 425]
![alpha-Terpineol](/CAS/GIF/98-55-5.gif)
98-55-5
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$21.00/25mL
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141-75-3
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$12.32/25G
![TERPINYL BUTYRATE](/CAS/GIF/2153-28-8.gif)
2153-28-8
32 suppliers
$259.75/2.5KG
![DL-Limonene](/CAS/GIF/138-86-3.gif)
138-86-3
323 suppliers
$22.39/100ML
![TERPINYL BUTYRATE](/CAS/GIF/2153-28-8.gif)
2153-28-8
32 suppliers
$259.75/2.5KG