ChemicalBook CAS DataBase List tert-butyl 2-(3-hydroxypropoxy)acetate

tert-butyl 2-(3-hydroxypropoxy)acetate synthesis

4synthesis methods

Product Name:tert-butyl 2-(3-hydroxypropoxy)acetate
CAS Number:930294-38-5
Molecular formula:C9H18O4
Molecular Weight:190.24

Acetic acid, 2-[3-(phenylmethoxy)propoxy]-, 1,1-dimethylethyl ester

930294-37-4
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930294-38-5
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Yield: 100%

Reaction Conditions:

with palladium on activated charcoal;hydrogen in ethanol at 20; for 5 h;

Steps:

1
Using ethanol as the solvent, adding C3 and palladium-carbon (10%) sequentially, using a hydrogen balloon to ventilate three times, and react at room temperature under hydrogen for 5 hours. After TLC detects that the reaction is complete, the reaction solution is filtered, and the filtrate is collected and distilled under reduced pressure to obtain C4, with a yield of about 100%.

References:

CN113214203, 2021, A Location in patent:Paragraph 0031; 0049-0051; 0053