ChemicalBook CAS DataBase List TERT-BUTYL 3-OXO-3-PHENYLPROPYLCARBAMATE

TERT-BUTYL 3-OXO-3-PHENYLPROPYLCARBAMATE synthesis

11synthesis methods

Product Name:TERT-BUTYL 3-OXO-3-PHENYLPROPYLCARBAMATE
CAS Number:333387-97-6
Molecular formula:C14H19NO3
Molecular Weight:249.31

24424-99-5 Synthesis

24424-99-5
827 suppliers
$13.50/25G

2038-57-5
168 suppliers
$14.14/1gm:

TERT-BUTYL 3-OXO-3-PHENYLPROPYLCARBAMATE

333387-97-6
18 suppliers
$373.00/100MG

Yield:333387-97-6 640 mg

Reaction Conditions:

Stage #1: 3-Phenylpropan-1-aminewith sodium hydroxide in acetonitrile;Inert atmosphere;Glovebox;
Stage #2: with sodium decatungstate;dihydrogen peroxide in acetonitrile;Inert atmosphere;Glovebox;
Stage #3: di-tert-butyl dicarbonateFurther stages;

References:

Schultz, Danielle M.;Lévesque, Fran?ois;DiRocco, Daniel A.;Reibarkh, Mikhail;Ji, Yining;Joyce, Leo A.;Dropinski, James F.;Sheng, Huaming;Sherry, Benjamin D.;Davies, Ian W. [Angewandte Chemie - International Edition,2017,vol. 56,# 48,p. 15274 - 15278][Angew. Chem.,2017,vol. 129,p. 15476 - 15480,5] Location in patent:supporting information

3303-84-2 Synthesis