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TERT-BUTYL (5-BROMO-1,3-BENZODIOXOL-4-YL)CARBAMATE synthesis

2synthesis methods
-

Yield:401811-77-6 96%

Reaction Conditions:

with diphenyl phosphoryl azide;triethylamine in 1,4-dioxane at 100; for 4 h;Curtius rearrangement;

References:

Plé, Patrick A.;Green, Tim P.;Hennequin, Laurent F.;Curwen, Jon;Fennell, Michael;Allen, Jack;Lambert-Van Der Brempt, Christine;Costello, Gerard [Journal of Medicinal Chemistry,2004,vol. 47,# 4,p. 871 - 887]

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