(TETRA-T-BUTYLPHTHALOCYANINATO)OXOVANADIUM(IV) synthesis
1synthesis methods
- Product Name:(TETRA-T-BUTYLPHTHALOCYANINATO)OXOVANADIUM(IV)
- CAS Number:95865-59-1
- Molecular formula:C48H48N8OV
- Molecular Weight:803.89
Yield:95865-59-1 46%
Reaction Conditions:
with hydrogenchloride;sodium hydroxide in neat (no solvent);reagents were reacted at 240-260°C for 2 h; mixt. was cooled to room temp. and then was boiled with 5% HCl and 5% NaOH, ppt. was washed with water and MeOH, chromd.; elem. anal.;
References:
Law, Kock-Yee [Inorganic Chemistry,1985,vol. 24,# 12,p. 1778 - 1781]