TETRAKIS(2-HYDROXYETHYL)AMMONIUM BROMIDE synthesis
- Product Name:TETRAKIS(2-HYDROXYETHYL)AMMONIUM BROMIDE
- CAS Number:4328-04-5
- Molecular formula:C8H20BrNO4
- Molecular Weight:274.15
121-44-8
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540-51-2
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$17.00/5g
4328-04-5
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$1715.18/25G
Yield:4328-04-5 98%
Reaction Conditions:
in toluene at 110; for 12 h;
Steps:
Typical synthesis procedure of hydroxyl-functionalized ionic liquids
General procedure: For the synthesis of N,N,N-triethyl-2-hydroxyethanaminium bromide (NEt3(HE)Br), a mixture of triethylamine (0.03mol), 2-bromoethanol (0.04mol) and dry toluene (10mL) was heated at 110°C for 12h in a 50ml single flask with vigorous stirring. Then the mixture was cooled down to room temperature, and a white solid formed rapidly. The resultant crude solid was filtered off, washed with acetone (5×20ml) and dried at 70°C for 12h under vacuum.
References:
Cheng, Weiguo;Xiao, Benneng;Sun, Jian;Dong, Kun;Zhang, Peng;Zhang, Suojiang;Ng, Flora T.T. [Tetrahedron Letters,2015,vol. 56,# 11,p. 1416 - 1419]
102-71-6
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$18.00/100g
540-51-2
235 suppliers
$17.00/5g
4328-04-5
11 suppliers
$1715.18/25G
540-51-2
235 suppliers
$17.00/5g
4328-04-5
11 suppliers
$1715.18/25G
25114-70-9
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540-51-2
235 suppliers
$17.00/5g
4328-04-5
11 suppliers
$1715.18/25G