ChemicalBook CAS DataBase List TRI-N-BUTYLISOCYANATOTIN

TRI-N-BUTYLISOCYANATOTIN synthesis

10synthesis methods

Product Name:TRI-N-BUTYLISOCYANATOTIN
CAS Number:681-99-2
Molecular formula:C13H27NOSn
Molecular Weight:332.07

2114-02-5 Synthesis

2114-02-5
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$6.00/10g

56-35-9 Synthesis

56-35-9
187 suppliers
$30.00/100g

Stannanamine, N,N'-methanetetraylbis[1,1,1-tributyl-

34885-41-1
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5035-65-4
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681-99-2
19 suppliers
$23.19/1g

Yield:34885-41-1 80.5%

Reaction Conditions:

in neat (no solvent);byproducts: water, ammonia; mixt. (molar ratio Sn-compd.:amidinothiourea=3:2) heating to 180-220°C (liberation of ammonia and water), exposition to vac.; fractional distn.;

References:

Gordetsov, A. S.;Latyaeva, V. N.;Bogdarin, Yu. A.;Boyarinov, G. A.;Dergunov, Yu. I. [Journal of general chemistry of the USSR,1982,vol. 52,p. 770 - 774][J.Gen.Chem.USSR (Engl.Transl.),1982,vol. 52,p. 885 - 890]

64-10-8 Synthesis