tributylstannyl methanesulfonate synthesis
2synthesis methods
- Product Name:tributylstannyl methanesulfonate
- CAS Number:13302-06-2
- Molecular formula:C13H30O3SSn
- Molecular Weight:385.15
Yield:13302-06-2 90%
Reaction Conditions:
in dichloromethane;to ClSnBu3 in CH2Cl2 is added AgSO3Me, mixt. is stirred at room temp. for 1 h; filtration, solvent is removed under reduced pressure, residue is heated at 0.01 mmHg, elem. anal.;
References:
Farah, Dan;Swami, Kamal;Kuivila, Henry G. [Journal of Organometallic Chemistry,1992,vol. 429,# 3,p. 311 - 334]
