Trifluoromethyl iodide synthesis
- Product Name:Trifluoromethyl iodide
- CAS Number:2314-97-8
- Molecular formula:CF3I
- Molecular Weight:195.91
421-83-0
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2314-97-8
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Yield:2314-97-8 86%
Reaction Conditions:
with sodium iodide in acetonitrile at 70; for 2 h;Inert atmosphere;
Steps:
5 Example 5
In a 20 mL tube, nitrogen was pumped 3 times, 1.7 g (0.01 mol) of the substrate represented by formula (II-5) was added, 5 mL of acetonitrile, 1.7 g of NaI (0.011 mol) was added, and the temperature was raised to 70 ° C. for 2 h.After the reaction, the product was collected by cooling with liquid nitrogen to obtain 1.5 g of a product represented by formula (I-5), with a yield of about 86% and a purity of> 98%.
References:
CN110759805,2020,A Location in patent:Paragraph 0112-0114
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2314-97-8
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