TRIMETHYLGALLIUM synthesis
- Product Name:TRIMETHYLGALLIUM
- CAS Number:1445-79-0
- Molecular formula:C3H9Ga
- Molecular Weight:114.83
75-24-1
153 suppliers
$54.50/100ml
13450-90-3
179 suppliers
$35.00/5g
1445-79-0
83 suppliers
$1248.00/25g
Yield: 90%
Reaction Conditions:
Reflux;
Steps:
1 Example 1
352 g (2.0 mol, 1.0 eq.) of GaCI3 (ex MCP) were poured into a 1 I two-neck round- bottom flask equipped with a distillation column, stirrer and a thermocouple. 447 g (6.2 mol, 3.1 eq.) TMAL were added dropwise to GaC . The mixture was gradually heated to reflux temperature. The distillate was collected into a cooled receiving flask (-5°C) with a top temperature of 56-58°C. TMG was isolated in a 90% yield (206 gram) with a purity of >99% based on 1H NMR analysis.
References:
AKZO NOBEL CHEMICALS INTERNATIONAL B.V.;TE NIJENHUIS, Marcellinus Antonius Maria;WOUDENBERG, RIchard Herman WO2019/115377, 2019, A1 Location in patent:Page/Page column 7
7440-55-3
141 suppliers
$39.20/50ml
74-88-4
342 suppliers
$15.00/10g
1445-79-0
83 suppliers
$1248.00/25g
75-24-1
153 suppliers
$54.50/100ml
1115-99-7
60 suppliers
$1170.00/10g
1445-79-0
83 suppliers
$1248.00/25g