TRIS[N,N-BIS(TRIMETHYLSILYL)AMIDE]CERIUM(III) synthesis
- Product Name:TRIS[N,N-BIS(TRIMETHYLSILYL)AMIDE]CERIUM(III)
- CAS Number:41836-21-9
- Molecular formula:C6H19CeNSi2
- Molecular Weight:301.51
1070-89-9
355 suppliers
$19.94/2g
76089-77-5
127 suppliers
$10.00/1g
41836-21-9
31 suppliers
$1480.50/25g
Yield:41836-21-9 82%
Reaction Conditions:
in tetrahydrofuran;(Ar); using Schlenk techniques; addn. of soln. of sodium bis(trimethylsilyl)amide in THF to Ce(OTf)3; reflux for ca. 4 h; cooling to room temp., removal of solvent in vac., extn. with pentane; filtration, evapn. of filtrate to dryness in vac., sublimation at 150°C and 1E-4 mmHg;
References:
Hitchcock, Peter B.;Hulkes, Alexander G.;Lappert, Michael F.;Li, Zhengning [Dalton Transactions,2004,# 1,p. 129 - 136]
7790-86-5
291 suppliers
$5.00/10g
40949-94-8
250 suppliers
$11.00/10g
41836-21-9
31 suppliers
$1480.50/25g
7790-86-5
291 suppliers
$5.00/10g
40949-94-8
250 suppliers
$11.00/10g
41836-21-9
31 suppliers
$1480.50/25g