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ChemicalBook CAS DataBase List Z,E-9,11-TETRADECADIENYL ACETATE

Z,E-9,11-TETRADECADIENYL ACETATE synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 95 percent / Amberlyst H-15 / hexane / 8 h / Ambient temperature
3: 94 percent / FeCl3 / diethyl ether / Ambient temperature
4: 1.) 1.6 M n-BuLi, 2.) ZnBr2, tetrakis triphenyl phosphine palladium (3percent) / 1.) Et2O, -60 deg C, 30 min, 2.) THF, RT

References:

Ramiandrasoa, F.;Tellier, F. [Synthetic Communications,1990,vol. 20,# 3,p. 333 - 344]

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