![](/CAS/GIF/14475-63-9.gif)
Zirconium hydroxide synthesis
- Product Name:Zirconium hydroxide
- CAS Number:14475-63-9
- Molecular formula:H4O4Zr
- Molecular Weight:159.25
ZrCl4 (aq)+ 4NaOH(aq) → Zr(OH)4 (s) + 4NaCl(aq)
![Zirconyl chloride octahydrate](/CAS/GIF/13520-92-8.gif)
13520-92-8
236 suppliers
$13.00/5g
![Ammonium hydroxide](/CAS/GIF/1336-21-6.gif)
1336-21-6
699 suppliers
$14.56/250ML
![Zirconium hydroxide](/CAS/GIF/14475-63-9.gif)
14475-63-9
223 suppliers
$38.89/100g
Yield:-
Reaction Conditions:
in water at 20; pH=9; for 6 h;
Steps:
1.1 Catalyst preparation
Appropriate amount of 0.1 M aqueous solution of zirconyl chloride (ZrOCl2·8H2O, Sinopharm Chemical Reagent Co., Ltd.) was added dropwise to ammonium hydroxide solution (NH4OH, 25%, Sinopharm Chemical Reagent Co., Ltd.) at room temperature under well-stirring.
The pH of the solution was controlled at 9, when a buoyant white powder immediately produced.
After stirring for 6 h at room temperature, the precipitate was evaporated in oil bath at 373 K, and then washed with deionized water five times, following by drying overnight at 383 K to generate a sample Zirconium hydroxide Zr(OH)4.
References:
Chen, Shiping;Wang, Weiming;Zhang, Yuanhua;Wei, Yucai;Fang, Weiping;Yang, Yiquan [Journal of Molecular Catalysis A: Chemical,2012,vol. 365,p. 60 - 65]
![Zirconium tetrachloride](/CAS/GIF/10026-11-6.gif)
10026-11-6
209 suppliers
$24.80/50g
![Sodium hydroxide](/CAS/20180808/GIF/1310-73-2.gif)
1310-73-2
1353 suppliers
$14.00/25g
![Zirconium hydroxide](/CAS/GIF/14475-63-9.gif)
14475-63-9
223 suppliers
$38.89/100g
![Ammonium hydroxide](/CAS/GIF/1336-21-6.gif)
1336-21-6
699 suppliers
$14.56/250ML
![Zirconium tetrachloride](/CAS/GIF/10026-11-6.gif)
10026-11-6
209 suppliers
$24.80/50g
![Zirconium hydroxide](/CAS/GIF/14475-63-9.gif)
14475-63-9
223 suppliers
$38.89/100g
![Water](/CAS/GIF/7732-18-5.gif)
7732-18-5
462 suppliers
$13.50/100ML
![Zirconium tetrachloride](/CAS/GIF/10026-11-6.gif)
10026-11-6
209 suppliers
$24.80/50g
![Zirconium hydroxide](/CAS/GIF/14475-63-9.gif)
14475-63-9
223 suppliers
$38.89/100g
![ZIRCONIUM NITRATE (ZIRCONYL)](/CAS/20211123/GIF/12372-57-5.gif)
12372-57-5
18 suppliers
inquiry
![Zirconium hydroxide](/CAS/GIF/14475-63-9.gif)
14475-63-9
223 suppliers
$38.89/100g