4-Chlorobiphenyl synthesis
- Product Name:4-Chlorobiphenyl
- CAS Number:2051-62-9
- Molecular formula:C12H9Cl
- Molecular Weight:188.65
106-46-7
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$10.00/5g
100-58-3
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$18.00/10ml
2051-62-9
131 suppliers
$35.00/250mg
Yield:2051-62-9 91.3%
Reaction Conditions:
with Ni(N,N'-bis(diphenylphosphino)-1,3-benzenediamine(-1H))Cl in tetrahydrofuran at 40; for 18 h;Schlenk technique;Inert atmosphere;Kumada Cross-Coupling;
Steps:
2.3. Typical procedure for the Kumada coupling reaction
General procedure: Aryl chloride (1.0 mmol), ArMgBr (1.5 mmol) in THF (2.0 mL), catalysts (2.0 mol%), were added to a Schlenk tube under an N2 atmosphere. The reaction was stirred at 40 °C for 12 h.
References:
Sun, Yunqiang;Li, Xiaoyan;Sun, Hongjian [Inorganica Chimica Acta,2014,vol. 415,p. 95 - 97]
106-46-7
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$10.00/5g
98-80-6
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$5.00/5g
2051-62-9
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$35.00/250mg
106-39-8
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$14.00/5g
780-69-8
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$9.00/25g
2051-62-9
131 suppliers
$35.00/250mg
106-39-8
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$14.00/5g
960-16-7
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$22.60/1g
2051-62-9
131 suppliers
$35.00/250mg
106-39-8
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$14.00/5g
591-51-5
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$45.89/50ml
2051-62-9
131 suppliers
$35.00/250mg