ChemicalBook--->CAS DataBase List--->1656-44-6

1656-44-6

1656-44-6 Structure

1656-44-6 Structure
IdentificationMore
[Name]

2,4-DINITROBENZENESULFONYL CHLORIDE
[CAS]

1656-44-6
[Synonyms]

2,4-DINITROBENZENESULFONYL CHLORIDE
2,4-DINITROBENZENESULPHONYL CHLORIDE
2,4-Dinitrobenzenesulfonylchl
2,4-dinitro-benzenesulfonylchlorid
Benzenesulfonyl chloride, 2,4-dinitro-
2,4-Dinitrobenzenesulfonic acid chloride
[EINECS(EC#)]

216-749-3
[Molecular Formula]

C6H3ClN2O6S
[MDL Number]

MFCD00007431
[Molecular Weight]

266.62
[MOL File]

1656-44-6.mol
Chemical PropertiesBack Directory
[Appearance]

yellow crystalline powder
[Melting point ]

101-103 °C (lit.)
[Boiling point ]

60-80 °C
[density ]

1.780
[Water Solubility ]

Reacts with water.
[Sensitive ]

Moisture Sensitive
[BRN ]

2147583
[CAS DataBase Reference]

1656-44-6(CAS DataBase Reference)
[EPA Substance Registry System]

Benzenesulfonyl chloride, 2,4-dinitro- (1656-44-6)
Safety DataBack Directory
[Hazard Codes ]

T,C
[Risk Statements ]

R34:Causes burns.
R65:Harmful: May cause lung damage if swallowed.
R48/23/24/25:Toxic: danger of serious damage to health by prolonged exposure through inhalation, in contact with skin and if swallowed .
R45:May cause cancer.
[Safety Statements ]

S53:Avoid exposure-obtain special instruction before use .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
S62:If swallowed, do not induce vomiting: seek medical advice immediately and show this container or label .
[RIDADR ]

UN 3261 8/PG 2
[WGK Germany ]

3
[F ]

21
[TSCA ]

Yes
[HazardClass ]

8
[PackingGroup ]

II
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

2,4-dinitrobenzene sulfonyl chloride(1656-44-6).msds
Hazard InformationBack Directory
[Chemical Properties]

yellow crystalline powder
[Uses]

2,4-Dinitrobenzenesulfonyl chloride was used to protect primary amines. It was used as starting reagent in the synthesis of tert-butyl 2-[(2,4-dinitrophenyl) sulfonyl]amino acetate.
[General Description]

2,4-Dinitrobenzenesulfonyl chloride causes the sulfonation of glycosylamines to yield N-glycosyl-2,4-dinitrobenzenesulfonamides.
[Purification Methods]

Crystallise the sulfonyl chloride from *benzene or *benzene/pet ether. [Beilstein 11 H 78, 11 IV 214.]
Spectrum DetailBack Directory
[Spectrum Detail]

2,4-DINITROBENZENESULFONYL CHLORIDE(1656-44-6)MS
2,4-DINITROBENZENESULFONYL CHLORIDE(1656-44-6)1HNMR
2,4-DINITROBENZENESULFONYL CHLORIDE(1656-44-6)13CNMR
2,4-DINITROBENZENESULFONYL CHLORIDE(1656-44-6)IR1
2,4-DINITROBENZENESULFONYL CHLORIDE(1656-44-6)Raman
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