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4'-Bromo-3'-nitroacetophenone

4'-Bromo-3'-nitroacetophenone structure

CAS No.: 18640-58-9

Chemical Name:: 4'-Bromo-3'-nitroacetophenone

Synonyms: NSC 111656;3-Nitro-4-bromoacetophenone;4-BROMO-3-NITROACETOPHENONE;4-bromo-3'-nitroacetophenone;4'-BROMO-3'-NITROACETOPHENONE;4'-Bromo-3'-nitroacetophenone;Acetophenone, 4'-bromo-3'-nitro-;4'-Bromo-3'-nitroacetophenone 97%;1-(4-BROMO-3-NITROPHENYL)ETHANONE;4'-Bromo-3'-nitroacetophenone >

CBNumber:: CB1465910

Molecular Formula:: C8H6BrNO3

Molecular Weight:: 244.04

MDL Number:: MFCD00016985

MOL File:: 18640-58-9.mol

Last updated:2024-07-22 10:05:22

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4'-Bromo-3'-nitroacetophenone Properties

Melting point	117-121 °C(lit.)
Boiling point	275.4℃
Density	1.637
refractive index	1.6090 (estimate)
Flash point	120.4℃
storage temp.	Sealed in dry,Room Temperature
form	Amorphous Powder
color	White to slightly yellow
BRN	2050098
InChI	InChI=1S/C8H6BrNO3/c1-5(11)6-2-3-7(9)8(4-6)10(12)13/h2-4H,1H3
InChIKey	YFVOFFKNHQTQQE-UHFFFAOYSA-N
SMILES	C(=O)(C1=CC=C(Br)C([N+]([O-])=O)=C1)C
CAS DataBase Reference	18640-58-9(CAS DataBase Reference)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H315-H319-H335

Precautionary statements

P261-P280a-P304+P340-P305+P351+P338-P405-P501a-P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313

Hazard Codes

Risk Statements

20/21/22

Safety Statements

24/25

WGK Germany

HS Code

29147000

NFPA 704

	0
1		0

4'-Bromo-3'-nitroacetophenone price More Price(35)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich	553662	4′-Bromo-3′-nitroacetophenone 97%	18640-58-9	5g	$50	2023-06-20	Buy
TCI Chemical	B3383	4'-Bromo-3'-nitroacetophenone >98.0%(GC)	18640-58-9	1g	$30	2024-03-01	Buy
TCI Chemical	B3383	4'-Bromo-3'-nitroacetophenone >98.0%(GC)	18640-58-9	5g	$90	2024-03-01	Buy
Alfa Aesar	B24469	4'-Bromo-3'-nitroacetophenone, 99%	18640-58-9	5g	$65.65	2024-03-01	Buy
Alfa Aesar	B24469	4'-Bromo-3'-nitroacetophenone, 99%	18640-58-9	25g	$210.65	2024-03-01	Buy

Product number	Packaging	Price	Buy
553662	5g	$50	Buy
B3383	1g	$30	Buy
B3383	5g	$90	Buy
B24469	5g	$65.65	Buy
B24469	25g	$210.65	Buy

4'-Bromo-3'-nitroacetophenone Chemical Properties,Uses,Production

Chemical Properties

white to slightly yellow amorphous powder

General Description

4′-Bromo-3′-nitroacetophenone is an electron deficient acetophenone derivative.

Synthesis

4'-Bromo-3'-nitroacetophenone is synthesised using 4'-Bromoacetophenone as a raw material by chemical reaction. The specific synthesis steps are as follows:
To fuming nitric acid (200 mL), l-(4- bromophenyl)-l-propanone (1-1) (40 g, 0.20 mol) was added while keeping the inside temperature of mixture at 5 to 10 0C. The reaction solution was stirred at this temperature for 30 minutes and then poured into ice. The precipitate was collected by filtration, washed with distilled water (25 mL x 2) and re-crystallized from methanol to give 1-2 (18 g, 37percent yield). 1H NMR (500 MHz, CDCl3) δ 8.38 (IH, d, J= 2.0 Hz), 7.99 (IH, dd, J= 8.2 Hz, 2.0 Hz), 7.86 (IH, d, J= 8.2Hz), 3.01 (2H, q, J= 7.1Hz), 1.25 (3H, t, J= 7.1Hz) ppm; LC-MS (ESI): m/z 244.0 (M+H)+.
4'-Bromo-3'-nitroacetophenone synthesis

4'-Bromo-3'-nitroacetophenone Preparation Products And Raw materials

Raw materials

Preparation Products

4-Acetyl-2-fluorobiphenyl 1-(4'-Methoxy-2-nitro-[1,1'-biphenyl]-4-yl)ethanone 1-(2-amino[1,1'-biphenyl]-4-yl)ethan-1-one 1-(2-Fluoro-4'-Methoxy-[1,1'-biphenyl]-4-yl)ethanone 1-(2-NITRO-BIPHENYL-4-YL)-ETHANONE

4'-Bromo-3'-nitroacetophenone Suppliers

Global( 194)Suppliers

Supplier	Tel	Email	Country	ProdList	Advantage
DSHare Pharmaceutical Science Technology Co.Ltd.	+8613962878782	wei.zhu@dshare.com.cn	China	42	58
Changzhou Ansciep Chemical Co., Ltd.	+86 519 86305871	sales@ansciepchem.com	CHINA	4241	58
Hubei xin bonus chemical co. LTD	86-13657291602	linda@hubeijusheng.com	CHINA	22963	58
Alchem Pharmtech,Inc.	8485655694	sales@alchempharmtech.com	United States	63687	58
CONIER CHEM AND PHARMA LIMITED	+8618523575427	sales@conier.com	China	49374	58
career henan chemical co	+86-0371-86658258 +8613203830695	factory@coreychem.com	China	29811	58
Antai Fine Chemical Technology Co.,Limited	18503026267	info@antaichem.com	CHINA	9636	58
Hefei TNJ Chemical Industry Co.,Ltd.	+86-0551-65418671 +8618949823763	sales@tnjchem.com	China	34553	58
Blocksynth Pharmaceutical Technology Co.,Ltd	0086-19817745290; +8619817745290	bd@blocksynth.com	China	5657	58
Shaanxi Dideu Medichem Co. Ltd	+86-029-89586680 +86-18192503167	1026@dideu.com	China	7724	58

Supplier	Advantage
DSHare Pharmaceutical Science Technology Co.Ltd.	58
Changzhou Ansciep Chemical Co., Ltd.	58
Hubei xin bonus chemical co. LTD	58
Alchem Pharmtech,Inc.	58
CONIER CHEM AND PHARMA LIMITED	58
career henan chemical co	58
Antai Fine Chemical Technology Co.,Limited	58
Hefei TNJ Chemical Industry Co.,Ltd.	58
Blocksynth Pharmaceutical Technology Co.,Ltd	58
Shaanxi Dideu Medichem Co. Ltd	58

View Lastest Price from 4'-Bromo-3'-nitroacetophenone manufacturers

Image	Update time	Product	Price	Min. Order	Purity	Supply Ability	Manufacturer
	2020-02-26	4′-Bromo-3′-nitroacetophenone 18640-58-9	US $0.00-0.00 / KG	100g	99.0%+	100 tons	Shaanxi Dideu Medichem Co. Ltd
	2020-02-14	4'-BROMO-3'-NITROACETOPHENONE 18640-58-9	US $7.00 / KG	1KG	99%	100KG	Career Henan Chemical Co

4′-Bromo-3′-nitroacetophenone
18640-58-9
US $0.00-0.00 / KG
99.0%+
Shaanxi Dideu Medichem Co. Ltd

4'-BROMO-3'-NITROACETOPHENONE
18640-58-9
US $7.00 / KG
99%
Career Henan Chemical Co

4'-Bromo-3'-nitroacetophenone Spectrum

4'-BROMO-3'-NITROACETOPHENONE(18640-58-9)MS 4'-BROMO-3'-NITROACETOPHENONE(18640-58-9)¹HNMR 4'-BROMO-3'-NITROACETOPHENONE(18640-58-9)IR1 4'-BROMO-3'-NITROACETOPHENONE(18640-58-9)IR2

18640-58-9(4'-Bromo-3'-nitroacetophenone)Related Search:

4'-Fluoro-3'-nitroacetophenone 4'-Bromoacetophenone 3-Nitrophenacylbromide 2-Bromo-4'-nitroacetophenone 2-BROMO-2'-NITROACETOPHENONE,-Bromo-2'-Nitroacetophenone

4'-BROMO-3'-NITROACETOPHENONE 3-nitro-4-bromopropiophenone 2-BROMO-5-NITROACETOPHENONE 5'-Bromo-2'-nitroacetophenone 3'-Bromo-4'-nitroacetophenone

4-BROMO-3'-NITROBENZOPHENONE A-BROMO-4-NITROACETOPHENONE HEXAMINE,α-Bromo-4-nitroacetophenone hexamine 2-Fluoro-3-Bromio-5-Nitro acetophenone Α-BROMO-P-NITROACETOPHENONE 2'-Bromo-α-nitroacetophenone

2-bromo-1-(4-bromo-3-nitrophenyl)ethanone 3-(4-bromo-3-nitrophenyl)-3-oxopropanenitrile 4-BROMO-3,5-DINITROBENZOPHENONE

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4'-BROMO-3'-NITROACETOPHENONE 4-BROMO-3-NITROACETOPHENONE 1-(4-BROMO-3-NITROPHENYL)ETHAN-1-ONE 1-(4-BROMO-3-NITROPHENYL)ETHANONE 3-Nitro-4-bromoacetophenone NSC 111656 4'-Bromo-3'-nitroacetophenone 97% Acetophenone, 4'-bromo-3'-nitro- Ethanone, 1-(4-bromo-3-nitrophenyl)- 4'-Bromo-3'-nitroacetophenone, 99+% 4'-bromo-3'-nitroacetophenone,1-(4-bromo-3-nitrophenyl)ethanone JRH-08504, 1-(4-Bromo-3-nitrophenyl)ethanone, 97% 2,4,6-trichloro-N-[(diphenylmethylene)amino]aniline 4'-Bromo-3'-nitroacetophenone > 4'-BROMO-3'-NITROACETOPHENONE USP/EP/BP 4'-Bromo-3'-nitroacetophenone 4-bromo-3'-nitroacetophenone 18640-58-9 18640-59-9 BrC6H3NO2COCH3 Organic Building Blocks Ketones C7 to C8 Carbonyl Compounds Building Blocks C7 to C8 Carbonyl Compounds Ketones Aromatic Ketones (substituted)