2,4-Dichloro-3-methyl-6-nitrophenol
- CAS No.
- 39549-27-4
- Chemical Name:
- 2,4-Dichloro-3-methyl-6-nitrophenol
- Synonyms
- 6-nitro-2,4-dichlor;2,4-dichloro-6-nitro-m-cresol;2,4-DICHLORO-6-NITRO-3-METHYLPHENOL;6-nitro-2,4-dichloro-3-methylphenol;2,4-Dichloro-3-Methyl-6-Nitro-Phenol;Phenol, 2,4-dichloro-3-methyl-6-nitro-
- CBNumber:
- CB3922709
- Molecular Formula:
- C7H5Cl2NO3
- Molecular Weight:
- 222.03
- MOL File:
- 39549-27-4.mol
- MSDS File:
- SDS
- Modify Date:
- 2024/2/27 10:07:46
| Melting point | 77-78 °C |
|---|---|
| Boiling point | 276.2±35.0 °C(Predicted) |
| Density | 1.587±0.06 g/cm3(Predicted) |
| storage temp. | 2-8°C |
| pka | 4.84±0.50(Predicted) |
| EPA Substance Registry System | Phenol, 2,4-dichloro-3-methyl-6-nitro- (39549-27-4) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |    GHS05,GHS07,GHS09 |
|---|---|
| Signal word | Danger |
| Hazard statements | H302-H315-H317-H318-H410 |
| Precautionary statements | P261-P264-P270-P272-P273-P280-P301+P312+P330-P302+P352-P305+P351+P338+P310-P333+P313-P391-P501 |
2,4-Dichloro-3-methyl-6-nitrophenol Chemical Properties,Uses,Production
Description
2,4-Dichloro-3-methyl-6-nitrophenol is a hydrocarbon solvent that is used in the synthesis of nitrotoluene. It is also used as an intermediate in the production of chlorinated phenols. The chlorination can be achieved by reacting 2,4-dichloro-3-methylphenol with hydrochloric acid and chlorine gas. The reaction with hydrochloric acid produces 2,4,6-trichlorophenol and 2,4-dichlorophenol. The reaction with chlorine gas produces 2,4,5-, and 3,5-, trichlorophenols. This chemical has been widely used in the production of organic solvents such as carbon tetrachloride and nitrobenzene.
Synthesis
2,4-Dichloro-3-methyl-6-nitrophenol 2 was prepared by KOH/H2O hydrolysis of a product mixture obtained from chlorination of p-nitrotoluene in the presence of a phase transfer catalyst. A 95–99% yield of 2 based on 2,3,6-trichloro-4-nitrotoluene, 4 (major chlorination product) was achieved in >95% purity[1].
References
[1] R. RAN C. P. A Practical Synthesis of 2,4-Dichloro-3-methyl-6-nitrophenol[J]. Synthetic Communications, 1993. DOI:10.1080/00397919308013809.
2,4-Dichloro-3-methyl-6-nitrophenol Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | Inquiry |
|---|---|---|---|---|---|
| ROSEWA HOLDING GROUP CO.,LIMITED | +86-023-62871537 | China | 2844 | 58 | Inquiry |
| Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 | China | 29798 | 60 | Inquiry |
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | China | 10311 | 58 | Inquiry |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | China | 49392 | 58 | Inquiry |
| SIMAGCHEM CORP | +86-13806087780 | China | 17367 | 58 | Inquiry |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | China | 34571 | 58 | Inquiry |
| Mainchem Co., Ltd. | +86-86-05926210733 +8618030271905 | China | 6572 | 58 | Inquiry |
| Amadis Chemical Company Limited | 571-89925085 | China | 131980 | 58 | Inquiry |
| DSL Chemicals Co.，Ltd | +86 21 6352 9955 | China | 6985 | 65 | Inquiry |
| Shanghai Jiegu Biotechnology Co., Ltd. | 021-51698675 | China | 4230 | 58 | Inquiry |
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