2-Aminoacetophenone hydrochloride
- CAS No.
- 5468-37-1
- Chemical Name:
- 2-Aminoacetophenone hydrochloride
- Synonyms
- 2-aMino-1-phenylethan-1-one hydrochloride;PHENACYLAMINE HYDROCHLORIDE;α-Aminoacetophenone;2-amino-acetophenonhydrochlo;2-aminophenone hydrochloride;2-amino-acetophenonhydrochloride;w-Aminoacetophenone hydrochloride;ω-aminoacetophenone hydrochloride;O-AMINOACETOPHENONE HYDROCHLORIDE;2-AMINOACETOPHENONE HYDROCHLORIDE
- CBNumber:
- CB6412186
- Molecular Formula:
- C8H10ClNO
- Molecular Weight:
- 171.62
- MOL File:
- 5468-37-1.mol
- MSDS File:
- SDS
- Modify Date:
- 2024/3/27 10:32:40
Melting point | 194 °C (dec.)(lit.) |
---|---|
storage temp. | Refrigerator (+4°C) |
solubility | DMSO (Slightly), Methanol (Slightly), Water (Slightly) |
form | Crystals |
color | Slightly yellow to beige |
BRN | 3563173 |
Stability | Hygroscopic |
InChI | InChI=1S/C8H9NO.ClH/c9-6-8(10)7-4-2-1-3-5-7;/h1-5H,6,9H2;1H |
InChIKey | CVXGFPPAIUELDV-UHFFFAOYSA-N |
SMILES | C(C1=CC=CC=C1)(=O)CN.[H]Cl |
CAS DataBase Reference | 5468-37-1(CAS DataBase Reference) |
EPA Substance Registry System | Ethanone, 2-amino-1-phenyl-, hydrochloride (5468-37-1) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
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Signal word | Warning | |||||||||
Hazard statements | H315-H319-H335 | |||||||||
Precautionary statements | P261-P280a-P304+P340-P305+P351+P338-P405-P501a | |||||||||
Hazard Codes | Xi | |||||||||
Risk Statements | 36/37/38 | |||||||||
Safety Statements | 37/39-26-24/25 | |||||||||
WGK Germany | 3 | |||||||||
RTECS | AM5940000 | |||||||||
TSCA | Yes | |||||||||
HazardClass | IRRITANT | |||||||||
HS Code | 29223990 | |||||||||
NFPA 704 |
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2-Aminoacetophenone hydrochloride price More Price(2)
2-Aminoacetophenone hydrochloride Chemical Properties,Uses,Production
Chemical Properties
Off-white crystalline
Synthesis
To a stirred solution of phenacyl bromide (1 mmol, 1 equiv) in diethyl ether (13 mL) was added hexamethylenetetramine (1 mmol, 1 equiv) all at once and the mixture was stirred for 12 h at room temperature. The resulting solid was filtered, washed with diethyl ether (15 mL), and dried under reduced pressure to afford the quaternary salt, which was next placed in a two-necked round-bottomed flask fitted with a reflux condenser, and EtOH (22 mL) was added to it. Concentrated HCl (0.6 mL) was added, and the mixture was refluxed for 3 h (solid formed). After cooling to room temperature, the solid was filtered, washed with EtOH (20 mL), and dried under vacuum to afford pure 2-Aminoacetophenone hydrochloride.
Purification Methods
Crystallise the salt from Me2CO /EtOH, EtOH/ Et2O, 2-propanol or 2-propanol and a little HCl (slowly after a fe
2-Aminoacetophenone hydrochloride Preparation Products And Raw materials
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Supplier | Advantage |
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GLR Innovations | 58 |
REDDY N REDDY PHARMACEUTICALS | 58 |
Rivashaa Agrotech Biopharma Pvt. Ltd. | 58 |
Denisco Chemicals Pvt Ltd | 58 |
HYPERSYNTH LIFE SCIENCES | 58 |
CLEARSYNTH LABS LTD. | 58 |
A.J Chemicals | 58 |
Alfa Aesar | 58 |
JUYE XIANDAI fine chemistry Co.,Ltd | 58 |
Capot Chemical Co.,Ltd. | 60 |
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