(S)-1-(4-Nitrophenyl)ethylamine hydrochloride
- CAS No.
- 57233-86-0
- Chemical Name:
- (S)-1-(4-Nitrophenyl)ethylamine hydrochloride
- Synonyms
- (+)-Nitresolve;(R)-A-METHYL-4-NITROBENZYLAMINE HCL;BenzeneMethanaMine, a-Methyl-4-nitro-;METHYL-4-NITROBENZYLAMINEHYDROCHLORIDE;(R)-(-)-1-(4-NITROPHENYL)-ETHYLAMINE HCL;1-(4-nitrophenyl)ethylamine hydrochloride;(R)-(-)-ALPHA-METHYL-4-NITROBENZYLAMINE HCL;(R)-4-NITROPHENYL-1-ETHYLAMINE HYDROCHLORIDE;(R)-4-Nitro-α-methylbenzylamine hydrochloride;(r)-α-methyl-4-nitrobenzylamine hydrochloride
- CBNumber:
- CB6465238
- Molecular Formula:
- C8H11ClN2O2
- Molecular Weight:
- 202.64
- MOL File:
- 57233-86-0.mol
- MSDS File:
- SDS
- Modify Date:
- 2022/11/11 11:01:00
| Melting point | 248-250 °C(lit.) |
|---|---|
| alpha | -6.5 º (c=1, 0.05N NaOH) |
| storage temp. | Inert atmosphere,Room Temperature |
| optical activity | [α]25/D +6.0°, c = 1 in 0.05 M NaOH |
| BRN | 3701567 |
| CAS DataBase Reference | 57233-86-0(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
| Hazard Codes | Xi |
| Risk Statements | 36/37/38 |
| Safety Statements | 26-37/39 |
| WGK Germany | 3 |
| F | 3-10 |
(S)-1-(4-Nitrophenyl)ethylamine hydrochloride Chemical Properties,Uses,Production
Purification Methods
To ensure dryness, the hydrochloride (ca 175 g) is extracted with EtOH (3x100mL) and evaporated to dryness (any residual H2O increases the solubility in EtOH and lowers the yield). The hydrochloride residue is triturated with absolute EtOH and dried in vacuo. The product is further purified by refluxing with absolute EtOH (200 mL for 83g) for 1hour, and cool to 10o to give 76.6g of hydrochloride m 243-245o(dec). The free base is prepared by dissolving in N NaOH, extracting with CH2Cl2 (3 x 500mL), drying (Na2CO3), filtering, evaporating and distilling it. It has m 27o, b 119-120o/0.5mm (105-107o/0.5mm, 157-159o/9mm, d 1.1764, n 1.5688, [] ±17.7o (neat) [Perry et al. Synthesis 492 1977,ORD: Nerdel & Liebig Justus Liebigs Ann Chem 621 142 1959]. [Beilstein 12 IV 2451.]
(S)-1-(4-Nitrophenyl)ethylamine hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
Global( 117)Suppliers
| Supplier | Tel | Country | ProdList | Advantage | Inquiry |
|---|---|---|---|---|---|
| career henan chemical co | +86-0371-86658258 +8613203830695 | China | 29901 | 58 | Inquiry |
| Changzhou Ditong Chemical Co.,Ltd | +86-0519-88299272 | China | 2169 | 58 | Inquiry |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | China | 49391 | 58 | Inquiry |
| Zhengzhou Alfa Chemical Co.,Ltd | +8618530059196 | China | 12915 | 58 | Inquiry |
| SIMAGCHEM CORP | +86-13806087780 | China | 17367 | 58 | Inquiry |
| Hefei TNJ Chemical Industry Co.,Ltd. | 0551-65418671 | China | 34571 | 58 | Inquiry |
| AFINE CHEMICALS LIMITED | +86-0571-85134551 | China | 15395 | 58 | Inquiry |
| Baoji Guokang Healthchem co.,ltd | +8615604608665 15604608665 | CHINA | 9427 | 58 | Inquiry |
| CD Chemical Group Limited | +8615986615575 | China | 20356 | 58 | Inquiry |
| Hebei Duling International Trade Co. LTD | +8617333973358 | China | 15440 | 58 | Inquiry |
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METHYL-4-NITROBENZYLAMINEHYDROCHLORIDE
(R)-4-Nitro-α-methylbenzylamine hydrochloride
Benzenemethanamine, .alpha.-methyl-4-nitro-, monohydrochloride, (.alpha.R)-
(r)-α-methyl-4-nitrobenzylamine hydrochloride
(R)-A-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE,97%
(R)-(-)-1-(4-NITROPHENYL)-ETHYLAMINE HCL
(R)-1-(4-NITROPHENYL)ETHYLAMINE HYDROCHLORIDE
(R)-4-NITROPHENYL-1-ETHYLAMINE HYDROCHLORIDE
(R)-(-)-ALPHA-METHYL-4-NITROBENZYLAMINE HCL
(R)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE
(R)-(+)-ALPHA-METHYL-4-NITROBENZYLAMMONIUM CHLORIDE
(R)-A-METHYL-4-NITROBENZYLAMINE HCL
(R)-(+)-A-METHYL 4-NITROBENZYLAMINE HYDROCHLORIDE
(S)-1-(4-Nitrophenyl)ethylamine hydrochloride
1-(4-nitrophenyl)ethylamine hydrochloride
(+)-Nitresolve
(R)-1-(4-nitrophenyl)ethanamine hydrochloride
BenzeneMethanaMine, a-Methyl-4-nitro-
(R)-alpha-Methyl-4-nitrobenzylaMine hydrochloride 97%
(R)-α-Methyl-4-nitrobenzylamine hydrochloride
Benzenemethanamine, α-methyl-4-nitro-, hydrochloride (1:1), (αR)-
(αR)-α-methyl-4-nitro-Benzenemethanamine hydrochloride (1:1)
(alphaR)-alpha-Methyl-4-nitro-benzenemethanamine HCl
57233-86-0
Chiral Resolving Reagents
Chiral Resolution Reagents
Asymmetric Synthesis