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ChemicalBook > Product Catalog >Organic Chemistry >Amides >Amino compound >TERT-BUTYL 4-BROMOBENZYLCARBAMATE

TERT-BUTYL 4-BROMOBENZYLCARBAMATE

TERT-BUTYL 4-BROMOBENZYLCARBAMATE Structure
CAS No.
68819-84-1
Chemical Name:
TERT-BUTYL 4-BROMOBENZYLCARBAMATE
Synonyms
N-BOC-4-broMobenzylaMine;4-Bromo-N-BOC-benzylamine;TERT-BUTYL 4-BROMOBENZYLCARBAMATE;tert-Butyl N-(4-bromobenzyl)carbamate;tert-Butyl 4-bromobenzylcarbamate 98%;tert-butyl N-[(4-bromophenyl)methyl]carbamate;N-(4-Bromobenzyl)carbamic acid tert-butyl ester;(4-BROMO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER;Carbamic acid, (4-bromophenyl)methyl-, 1,1-dimethylethyl ester;N-[(4-Bromophenyl)methyl]-carbamic acid 1,1-dimethylethyl ester
CBNumber:
CB6838195
Molecular Formula:
C12H16BrNO2
Molecular Weight:
286.16
MOL File:
68819-84-1.mol
Modify Date:
2024/1/9 16:41:59
Request For Quotation

TERT-BUTYL 4-BROMOBENZYLCARBAMATE Properties

Melting point 86-88℃
Boiling point 374.3±25.0 °C(Predicted)
Density 1.319±0.06 g/cm3(Predicted)
storage temp. Sealed in dry,Room Temperature
form solid
pka 12.05±0.46(Predicted)
color Off-white

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS07
Signal word  Warning
Hazard statements  H319-H335-H302+H312+H332-H315
Precautionary statements  P280-P301+P312-P362+P364
Hazard Codes  Xn
Risk Statements  22
HS Code  2924297099

TERT-BUTYL 4-BROMOBENZYLCARBAMATE Chemical Properties,Uses,Production

Synthesis

Tert-Butyl 4-bromobenzylcarbamate is prepared by the reaction of di-tert-butyl dicarbonate and 4-bromobenzylamine hydrochloride. The specific synthesis steps are as follows:
To a stirred suspension of 4-bromo-benzylamine hydrochloride (968mg, 4.35mmol) and triethylamine (0.666ml, 4.79mmol) in chloroform (15ml) was added di-tert-butyldicarbonate (949mg, 4.35mmol). The resulting solution was stirred at ambient temperature for 2h and then diluted with DCM (40ml). The organic solution was washed sequentially with 10% aqueous citric acid (40ml) and brine (40ml). The organic phase was dried over anhydrous magnesium sulfate and the filtrate evaporated at reduced pressure to afford Tert-Butyl 4-bromobenzylcarbamate (1.23g, 99%). 1H NMR 7.48-7.43 (2H, m), 7.18 (2H, d, 8.4), 4.84 (1H, br s), 4.27 (2H, d, 5.7), 1.46 (9H, s).
TERT-BUTYL 4-BROMOBENZYLCARBAMATE synthesis

TERT-BUTYL 4-BROMOBENZYLCARBAMATE Preparation Products And Raw materials

Raw materials

Preparation Products

tert-Butyl 4-ethynylbenzylcarbamate (4-IODO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER [1-(4-BROMO-PHENYL)-ETHYL]-CARBAMIC ACID TERT-BUTYL ESTER 4-AMINOMETHYLPHENYLBORONIC ACID, PINACOL ESTER, HCL (4-BROMO-BENZYL)-METHYL-CARBAMIC ACID TERT-BUTYL ESTER
Methyl 3-(4-((tert-butoxycarbonylaMino)Methyl)phenylsulfonyl)propanoate
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TERT-BUTYL 4-BROMOBENZYLCARBAMATE Suppliers

Global( 113)Suppliers
Supplier Tel Country ProdList Advantage Inquiry
A.J Chemicals 91-9810153283 New Delhi, India 6124 58 Inquiry
career henan chemical co +86-0371-86658258 +8613203830695 China 29826 58 Inquiry
Hubei Ipure Biology Co., Ltd +8613367258412 China 10326 58 Inquiry
Blocksynth Pharmaceutical Technology Co.,Ltd 0086-19817745290; +8619817745290 China 5660 58 Inquiry
Labnetwork lnc. +86-27-50766799 +8618062016861 China 19994 58 Inquiry
Hefei TNJ Chemical Industry Co.,Ltd. 0551-65418684 +8618949823763 China 25363 58 Inquiry
LEAP CHEM CO., LTD. +86-852-30606658 China 24738 58 Inquiry
Aromsyn Co., Ltd. +86-0571-85585865 +8613336024896 China 19185 58 Inquiry
Wuhan Konberd Biotech Co., Ltd +undefined18986093962 China 1376 58 Inquiry
Aceschem Inc. +1-817863-6948 +1-（817）863-6948 United States 19639 58 Inquiry
Supplier Advantage
A.J Chemicals 58
career henan chemical co 58
Hubei Ipure Biology Co., Ltd 58
Blocksynth Pharmaceutical Technology Co.,Ltd 58
Labnetwork lnc. 58
Hefei TNJ Chemical Industry Co.,Ltd. 58
LEAP CHEM CO., LTD. 58
Aromsyn Co., Ltd. 58
Wuhan Konberd Biotech Co., Ltd 58
Aceschem Inc. 58

68819-84-1(TERT-BUTYL 4-BROMOBENZYLCARBAMATE)Related Search:

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TERT-BUTYL 4-BROMOBENZYLCARBAMATE Carbamic acid, (4-bromophenyl)methyl-, 1,1-dimethylethyl ester (4-BROMO-BENZYL)-CARBAMIC ACID TERT-BUTYL ESTER 4-Bromo-N-BOC-benzylamine N-(4-Bromobenzyl)carbamic acid tert-butyl ester tert-Butyl N-(4-bromobenzyl)carbamate Carbamic acid, N-[(4-bromophenyl)methyl]-, 1,1-dimethylethyl ester tert-Butyl 4-bromobenzylcarbamate 98% tert-butyl N-[(4-bromophenyl)methyl]carbamate N-BOC-4-broMobenzylaMine N-[(4-Bromophenyl)methyl]-carbamic acid 1,1-dimethylethyl ester 68819-84-1 amine|alkyl bromide| carboxylic ester