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tert-Butyl N-hydroxycarbamate

CAS No.: 36016-38-3

Chemical Name:: tert-Butyl N-hydroxycarbamate

Synonyms: tert-Butyl hydroxycarbamate;N-BOC-HYDROXYLAMINE;BOC-NH-OH;BOC-HNOH;N-Boc-hydroxyL;BOC hydroxylamine;N-Boc-Hydroxyamine;N-hydroxycarbamate;N-T-BOC HYDROXYLAMINE;LABOTEST-BB LT00233206

CBNumber:: CB7274369

Molecular Formula:: C5H11NO3

Molecular Weight:: 133.15

MOL File:: 36016-38-3.mol

MSDS File:: SDS

Modify Date:: 2024/5/21 9:37:49

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tert-Butyl N-hydroxycarbamate Properties

Melting point	53-55 °C (lit.)
Boiling point	245.66°C (rough estimate)
Density	1.2510 (rough estimate)
refractive index	1.4120 (estimate)
storage temp.	2-8°C
solubility	Chloroform, Methanol
form	Crystalline Powder
pka	9.31±0.23(Predicted)
color	White to light pink
Water Solubility	Slightly soluble in water.
Sensitive	Moisture Sensitive
BRN	1756546
InChI	InChI=1S/C5H11NO3/c1-5(2,3)9-4(7)6-8/h8H,1-3H3,(H,6,7)
InChIKey	DRDVJQOGFWAVLH-UHFFFAOYSA-N
SMILES	C(OC(C)(C)C)(=O)NO
CAS DataBase Reference	36016-38-3(CAS DataBase Reference)

SAFETY

Risk and Safety Statements

Symbol(GHS)

GHS07

Signal word

Warning

Hazard statements

H315-H319-H335

Precautionary statements

P280-P261

Safety Statements

22-24/25

WGK Germany

HS Code

29280090

NFPA 704

	1
0		0

tert-Butyl N-hydroxycarbamate price More Price(7)

Manufacturer	Product number	Product description	CAS number	Packaging	Price	Updated	Buy
Sigma-Aldrich(India)	226157	N-Boc-hydroxylamine ≥98%	36016-38-3	1G	₹2792.85	2022-06-14	Buy
Sigma-Aldrich(India)	226157	N-Boc-hydroxylamine ≥98%	36016-38-3	5G	₹8681.65	2022-06-14	Buy
ALFA India	ALF-A10349-14	N-Boc-hydroxylamine, 98+%	36016-38-3	25g	₹7700	2022-05-26	Buy
TCI Chemicals (India)	H0848	tert-Butyl N-Hydroxycarbamate min. 97.0 %	36016-38-3	5G	₹3100	2022-05-26	Buy
TCI Chemicals (India)	H0848	tert-Butyl N-Hydroxycarbamate min. 97.0 %	36016-38-3	25G	₹7700	2022-05-26	Buy

Product number	Packaging	Price	Buy
226157	1G	₹2792.85	Buy
226157	5G	₹8681.65	Buy
ALF-A10349-14	25g	₹7700	Buy
H0848	5G	₹3100	Buy
H0848	25G	₹7700	Buy

tert-Butyl N-hydroxycarbamate Chemical Properties,Uses,Production

Chemical Properties

White to light pink crystalline powder

Uses

tert-Butyl N-hydroxycarbamate is used in the preparation of azridines by cycloaddition of azides with nitroso Diels-Alder adducts.

Synthesis Reference(s)

Journal of the American Chemical Society, 81, p. 955, 1959 DOI: 10.1021/ja01513a049
Tetrahedron Letters, 24, p. 231, 1983 DOI: 10.1016/S0040-4039(00)81372-6

Synthesis

A suspension of NH2OH·HCl (9.7 g, 140mmol) and K2CO3 (9.7 g, 700 mmol) in Et2O (60 mL) and H2O (2 mL)was stirred for about 1 h at r.t. with evolution of CO2 gas. A solution of Boc2O (20.0 g, 92 mmol) in Et2O (40 mL) was then added dropwise at 0 °C, and the suspension was stirred at r.t for 12 h. The organic phase was decanted, and the solid was washed with Et2O (3 × 30 mL). The combined organic layers were concentrated, and the residue was recrystallized from cyclohexane/toluene to afford the desired product tert-butyl N-hydroxycarbamate as a white solid.

tert-Butyl N-hydroxycarbamate Preparation Products And Raw materials

Raw materials

Preparation Products

tert-butyl hydroxy(methyl)carbamate N-(TERT-BUTOXYCARBONYL)-2-BROMOANILINE 1-Boc-2-isopropylhydrazine tert-Butyl (Mesitylsulfonyl)oxycarbaMate TERT-BUTYL N-(TERT-BUTOXYCARBONYLOXY)CARBAMATE

O-(4-nitrobenzoyl)hydroxylamine 2-(TERT-BUTOXYCARBONYLAMINO)PYRIDINE tert-butyl (2,4-dinitrophenoxy)carbamate

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tert-Butyl N-hydroxycarbamate Suppliers

Global( 392)Suppliers

Supplier	Tel	Country	ProdList	Advantage	Inquiry
BTC pharm India	+918790379245	AndhraPradesh, India	1269	58	Inquiry
GLR Innovations	+91 9891111994	New Delhi, India	4542	58	Inquiry
SUMUKHA LIFESCIENCES	+919000487488	Hyderabad, India	200	58	Inquiry
NSR Laboratories Pvt. Ltd.	+91-9866989891 +91-9000457345	Hyderabad, India	196	58	Inquiry
SIRI LIFE SCIENCES	+91-9000234689 +91-9000234689	Hyderabad, India	177	58	Inquiry
Sris Synthesis Pvt Ltd.,	+91-9989522441 +91-9989522441	Hyderabad, India	282	58	Inquiry
SYNOVA CHEMICALS	+91-9920741772 +91-9920741772	Mumbai, India	428	58	Inquiry
PRODIGIOUS LIFE SCIENCES	+91-9177472555 +91-9177472555	Hyderabad, India	236	58	Inquiry
AMINO ORGANICS	+919866989891	Hyderabad, India	275	58	Inquiry
JSK Chemicals	+919879767970	Gujarat, India	3756	58	Inquiry

Supplier	Advantage
BTC pharm India	58
GLR Innovations	58
SUMUKHA LIFESCIENCES	58
NSR Laboratories Pvt. Ltd.	58
SIRI LIFE SCIENCES	58
Sris Synthesis Pvt Ltd.,	58
SYNOVA CHEMICALS	58
PRODIGIOUS LIFE SCIENCES	58
AMINO ORGANICS	58
JSK Chemicals	58

tert-Butyl N-hydroxycarbamate Spectrum

tert-Butyl N-hydroxycarbamate(36016-38-3)MS tert-Butyl N-hydroxycarbamate(36016-38-3)¹HNMR tert-Butyl N-hydroxycarbamate(36016-38-3)¹³CNMR tert-Butyl N-hydroxycarbamate(36016-38-3)IR1 tert-Butyl N-hydroxycarbamate(36016-38-3)IR2 tert-Butyl N-hydroxycarbamate(36016-38-3)Raman

36016-38-3(tert-Butyl N-hydroxycarbamate)Related Search:

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N-Boc-hydroxylamine, >=98% N-tert-Butoxycarbonylhydroxylamine, 98+% N-(tert-Butoxycarbonyl)hydroxylamine~tert-ButylN-hydroxycarbamate N-(T-BUTOXYCARBONYL)-HYDROXYLAMINE N-T-BOC HYDROXYLAMINE N-HYDROXYCARBAMIC ACID TERT-BUTYL ESTER TERT-BUTYL N-HYDROXYCARBAMATE 99.0% N-Boc-Hydroxyamine T-BUTYL N-HYDROXYCARBOMATE (N-BOC HYDROXYLAMINE) T-BUTYL N-HYDROXYCARBOMATE PNB(4R,5S,6S)-3-(diphenyloxy)phosphoryloxy-6[(1R)-1-hydoxyethyl]-4-methyl -7-oxo-1-azabicyclo[3,2,0]hept-2-ene-2-caboxylate(MAP or MVP) N-t-Butyloxycarbonyl-hydroxylamine N-Boc-hydroxylamine N-(tert-Butoxycarbonyl)hydroxylamine N-Hydroxycarbamic Acid tert-Butyl Ester N-hydroxy-, 1,1-dimethylethyl ester Carbamic acid, hydroxy-, 1,1-dimethylethyl ester (Hydroxyamino)formic acid tert-butyl ester tert-Butyl N-hydroxycarbamate BOC-HNOH T-BUTYL N-HYDROXYCARBAMATE TERT-BUTYL N-HYDROXYCARBAMATE LABOTEST-BB LT00233206 N-(TERT-BUTYLOXYCARBONYL)HYDROXYLAMINE N-TERT-BUTOXYCARBONYLHYDROXYLAMINE BOC-Hydroxylamine Tert-Butyl N-hydroxycarbamate Carbamic acid,N-hydroxy-, 1,1-dimethylethyl ester N-Boc-hydroxylamine≥ 99% (HPLC) N-tert-BOC-Hydroxylamine for synthesis N-(tert-Butoxycarbonyl)hyd BOC hydroxylamine 4-hydroxy-2-[[(2-methylpropan-2-yl)oxy-oxomethyl]amino]butanoic acid n-hydroxycarbamate tert butyl ester tert-ButylN-Hydroxycarbamate> N-Boc-hydroxyL N-hydroxycarbamate ert-ButylN-hydroxycarbamate N-tert-Boc-Hydroxylamine N-BOC-HYDROXYLAMINE tert-Butyl hydroxycarbamate BOC-NH-OH (t-Butoxycarbonyl)-hydroxylamine 36016-38-3 C5H11O3N CH33COCONHOH Hydroxylamines Hydroxylamines (N-Substituted) Building Blocks Organic Building Blocks Nitrogen Compounds Protected Amines Hydroxylamines Hydroxylamines (N-Substituted) Naphthyridine,Quinoline API intermediates INTERMEDIATESOFMEROPENAM 1