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2-Iodo-4-methoxy-1-nitrobenzene

2-Iodo-4-methoxy-1-nitrobenzene Structure
CAS No.
214279-40-0
Chemical Name:
2-Iodo-4-methoxy-1-nitrobenzene
Synonyms
3-Iodo-4-nitroanisol;4-NITRO-3-IODOANISOLE;3-IODO-4-NITROANISOLE;3-Iodo-4-nitroanisole,97%;3-Iodo-4-nitroanisole, 97% 5GR;2-Iodo-4-Methoxy-1-nitrobenzene;Benzene, 2-iodo-4-methoxy-1-nitro-;2-Iodo-4-methoxy-1-nitrobenzene, 3-Iodo-4-nitrophenyl methyl ether
CBNumber:
CB7397572
Molecular Formula:
C7H6INO3
Molecular Weight:
279.03
MOL File:
214279-40-0.mol
Modify Date:
2024/5/10 8:45:28

2-Iodo-4-methoxy-1-nitrobenzene Properties

Melting point 68-73 °C
Boiling point 352.1±27.0 °C(Predicted)
Density 1.9259 (estimate)
storage temp. Keep in dark place,Sealed in dry,Room Temperature
form Crystals or Crystalline Powder
color Yellow to orange-brown
InChI InChI=1S/C7H6INO3/c1-12-5-2-3-7(9(10)11)6(8)4-5/h2-4H,1H3
InChIKey NLTAHTYBZZSCIT-UHFFFAOYSA-N
SMILES C1([N+]([O-])=O)=CC=C(OC)C=C1I

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P305+P351+P338
Hazard Codes  Xn
Risk Statements  36-33-20/21/22
Safety Statements  36/37-22
HS Code  29093090

2-Iodo-4-methoxy-1-nitrobenzene Chemical Properties,Uses,Production

Chemical Properties

yellow to orange-brown crystals or

Synthesis

Silak reaction tube equipped with a magnetic stirrer was charged with 6.2 mg of silver sulfate,21.8 mg of copper acetate, 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline,39.4 mg of 2-nitro-5-methoxybenzoic acid and 45 mg of sodium iodide4 mL of dimethyl sulfoxide. The reaction was heated at 160 ° C for 24 hours with oxygen. After the reaction, distilled water was added to quench the reaction. Extraction with ethyl acetate 3 times, each time 10mL. The combined organic phases are concentrated; 35.2 mg of 2-Iodo-4-methoxy-1-nitrobenzene was obtained in a yield of 63 percent.

2-Iodo-4-methoxy-1-nitrobenzene Preparation Products And Raw materials

Raw materials

Preparation Products

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3-IODO-4-NITROANISOLE 4-NITRO-3-IODOANISOLE 3-Iodo-4-nitroanisole,97% 2-Iodo-4-Methoxy-1-nitrobenzene 3-Iodo-4-nitroanisole, 97% 5GR 2-Iodo-4-methoxy-1-nitrobenzene, 3-Iodo-4-nitrophenyl methyl ether 3-Iodo-4-nitroanisol Benzene, 2-iodo-4-methoxy-1-nitro- 214279-40-0 Aromatic Ethers