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N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE

N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE Structure
CAS No.
60394-88-9
Chemical Name:
N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE
Synonyms
Arnottianamide;N-[6-(2-hydroxy-3,4-dimethoxyphenyl)benzo[f][1,3]benzodioxol-5-yl]-N-methylformamide;N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE;Formamide, N-[6-(2-hydroxy-3,4-dimethoxyphenyl)naphtho[2,3-d]-1,3-dioxol-5-yl]-N-methyl-;N-[6-(2-HYDROXY-3,4-DIMETHOXY-PHENYL)-NAPHTHO[2,3-'D][1,3]DIOXOL-5-YL]-N-METHYL-FORMAMIDE
CBNumber:
CB9237645
Molecular Formula:
C21H19NO6
Molecular Weight:
381.38
MOL File:
60394-88-9.mol
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N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE Properties

Melting point 264-267 °C
Boiling point 573.8±50.0 °C(Predicted)
Density 1.353±0.06 g/cm3(Predicted)
pka 8.50±0.40(Predicted)

N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE Chemical Properties,Uses,Production

Description

Arnottianamide occurs in Xanthoxylum arnottianum and, in trace amounts, in X. cuspidatum. It crystallizes as colourless prisms from EtOH and gives an ultraviolet spectrum in ethanol with absorption maxima at 236 and 332 nm and shoulders at 280 and 324 nm. The structure has been elucidated from chemical and spectro-scopic data and confirmed by its preparation from chelerythrine chloride by a Baeyer-Villiger type oxidation of the irnmonium group. Treatment with LiA1H4 gives the deoxo derivative as colourless prisms, m.p. 200-2°C, forming a crystalline methyl derivative, m.p. l66.5-168.5°C.

References

Ishii et al., Tetrahedron Lett., 1203 (1976)

N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE Suppliers

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Fluorochem Ltd. 74
3B Scientific Corporation 56
3B Scientific Corporation 47
Fluorochem Ltd 65
Shanghai PI Chemicals Ltd. 56
UK GREEN SCIENTIFIC CO.,LIMITED 47
ETA SCIENTIFIC Co.,Ltd 34
CARBONE SCIENTIFIC CO.,LTD 30
Oakwood Products, Inc. 74
Nanning Saifir Biotechnology Co., Ltd. 58

60394-88-9(N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE)Related Search:

N-Methylformamide
Arnottianamide N-[6-(2-HYDROXY-3,4-DIMETHOXY PHENYL)NAPHTHO[2,3-D][1,3]DIOXOL-5-YL]-N-METHYLFORMAMIDE N-[6-(2-HYDROXY-3,4-DIMETHOXY-PHENYL)-NAPHTHO[2,3-'D][1,3]DIOXOL-5-YL]-N-METHYL-FORMAMIDE N-[6-(2-hydroxy-3,4-dimethoxyphenyl)benzo[f][1,3]benzodioxol-5-yl]-N-methylformamide Formamide, N-[6-(2-hydroxy-3,4-dimethoxyphenyl)naphtho[2,3-d]-1,3-dioxol-5-yl]-N-methyl- 60394-88-9 C21H19NO6