2-[[(1,1-디메틸에톡시)카르보닐]아미노]-4-피리딘카르복실산메틸에스테르
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2-[[(1,1-디메틸에톡시)카르보닐]아미노]-4-피리딘카르복실산메틸에스테르 속성
- 녹는점
- 75.1~75.2℃
- 끓는 점
- 325.5±27.0 °C(Predicted)
- 밀도
- 1.203±0.06 g/cm3(Predicted)
- 저장 조건
- under inert gas (nitrogen or Argon) at 2-8°C
- 산도 계수 (pKa)
- 12.12±0.70(Predicted)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
HS 번호 | 2922390090 |
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그림문자(GHS): | |||||||||||||||
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신호 어: | Warning | ||||||||||||||
유해·위험 문구: |
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예방조치문구: |
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2-[[(1,1-디메틸에톡시)카르보닐]아미노]-4-피리딘카르복실산메틸에스테르 C화학적 특성, 용도, 생산
Synthesis
A 500 mL round bottomed flask was charged with methyl 2-aminoisonicotinate (5.0 g, 32.9 mmol) and suspended in t-BuOH (200 mL). To this stirring solution was added di-tert-butyl dicarbonate (7.53 g, 34.5 mmol). The flask was vented and placed in an oil bath preheated to 50°C. The reaction mixture was let stir overnight. After 22 hours LCMS showed near complete conversion of starting material. The mixture was cooled to room temperature and filtered. The material was taken on without any further purification. Yield 5.93 g of white solid, Methyl 2-(Boc-amino)isonicotinate. 1H NMR (400 MHz, DMSO-d6) δ ppm 10.14 (1H, s), 8.43 (1H, dd, J=5.02, 0.75 Hz), 8.33 (1H, s), 7.45 (1H, dd, J=5.02, 1.51 Hz), 3.89 (3H, s), 1.48 (9H, s).2-[[(1,1-디메틸에톡시)카르보닐]아미노]-4-피리딘카르복실산메틸에스테르 준비 용품 및 원자재
원자재
준비 용품
2-[[(1,1-디메틸에톡시)카르보닐]아미노]-4-피리딘카르복실산메틸에스테르 공급 업체
글로벌( 69)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
---|---|---|---|---|---|
Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 |
sales@capotchem.com | China | 29798 | 60 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 |
ivan@atkchemical.com | China | 32835 | 60 |
Accela ChemBio Inc. | +1-858-6993322 |
info@accelachem.com | United States | 19751 | 58 |
Alchem Pharmtech,Inc. | 8485655694 |
sales@alchempharmtech.com | United States | 63711 | 58 |
Fuxin Pharmaceutical | +86-021-021-50872116 +8613122107989 |
contact@fuxinpharm.com | China | 10297 | 58 |
Blocksynth Pharmaceutical Technology Co.,Ltd | 0086-19817745290; +8619817745290 |
bd@blocksynth.com | China | 5660 | 58 |
Wuhan Konberd Biotech Co., Ltd | +undefined18986093962 |
admin@konberdbio.com | China | 1376 | 58 |
Aladdin Scientific | +1-+1(833)-552-7181 |
sales@aladdinsci.com | United States | 52927 | 58 |
Suzhou ARTK Medchem Co., Ltd. | +86-512-68323658 +86-18168183658 |
sales1@artkmedchem.com | China | 39010 | 58 |
Amadis Chemical Company Limited | 571-89925085 |
sales@amadischem.com | China | 131980 | 58 |