ChemicalBook >> CAS DataBase List >>Methyl 2-(Boc-amino)isonicotinate
Methyl 2-(Boc-amino)isonicotinate
- CAS No.
- 639091-75-1
- Chemical Name:
- Methyl 2-(Boc-amino)isonicotinate
- Synonyms
- Methyl 2-(Boc-amino)isonicotinate;2-Boc-amino-isonicotinic acid methyl ester;Methyl 2-((tert-butoxycarbonyl)aMino)isonicotinate;2-tert-Butoxycarbonylamino-isonicotinic acid methyl ester;methyl 2-(tert-butoxycarbonylamino)pyridine-4-carboxylate;Methyl 2-[(2-methylpropan-2-yl)oxycarbonylamino]pyridine-4-carboxylate;2-[[(1,1-Dimethylethoxy)carbonyl]amino]-4-pyridinecarboxylic acidmethylester;4-Pyridinecarboxylic acid, 2-[[(1,1-diMethylethoxy)carbonyl]aMino]-, Methyl ester
- CBNumber:
- CB02499400
- Molecular Formula:
- C12H16N2O4
- Molecular Weight:
- 252.27
- MDL Number:
- MFCD11504796
- MOL File:
- 639091-75-1.mol
- MSDS File:
- SDS
Last updated:2023-07-10 08:28:02
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302 |
| Precautionary statements | P264-P270-P301+P312-P330 |
| HS Code | 2922390090 |
Methyl 2-(Boc-amino)isonicotinate price More Price(21)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | M295635 | Methyl2-(Boc-amino)isonicotinate | 639091-75-1 | 250mg | $55 | 2021-12-16 | Buy |
| Matrix Scientific | 018214 | 2-(2,2-Dimethyl-propionylamino)-isonicotinic acidmethyl ester | 639091-75-1 | 500mg | $116 | 2021-12-16 | Buy |
| Matrix Scientific | 118101 | Methyl 2-((tert-butoxycarbonyl)amino)isonicotinate | 639091-75-1 | 5g | $301 | 2021-12-16 | Buy |
| SynQuest Laboratories | 4H58-1-8C | Methyl 2-((tert-butoxycarbonyl)amino)isonicotinate | 639091-75-1 | 5G | $356 | 2021-12-16 | Buy |
| AK Scientific | Y6341 | Methyl2-(tert-butoxycarbonylamino)isonicotinate | 639091-75-1 | 10g | $370 | 2021-12-16 | Buy |
Methyl 2-(Boc-amino)isonicotinate Chemical Properties,Uses,Production
Synthesis
A 500 mL round bottomed flask was charged with methyl 2-aminoisonicotinate (5.0 g, 32.9 mmol) and suspended in t-BuOH (200 mL). To this stirring solution was added di-tert-butyl dicarbonate (7.53 g, 34.5 mmol). The flask was vented and placed in an oil bath preheated to 50°C. The reaction mixture was let stir overnight. After 22 hours LCMS showed near complete conversion of starting material. The mixture was cooled to room temperature and filtered. The material was taken on without any further purification. Yield 5.93 g of white solid, Methyl 2-(Boc-amino)isonicotinate. 1H NMR (400 MHz, DMSO-d6) δ ppm 10.14 (1H, s), 8.43 (1H, dd, J=5.02, 0.75 Hz), 8.33 (1H, s), 7.45 (1H, dd, J=5.02, 1.51 Hz), 3.89 (3H, s), 1.48 (9H, s).
Synthesis of Methyl 2-(Boc-amino)isonicotinate from Methyl 2-aminopyridine-4-carboxylate and Di-tert-butyl dicarbonate
Methyl 2-(Boc-amino)isonicotinate Preparation Products And Raw materials
Raw materials
Preparation Products
Global( 69)Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
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| Shijiazhuang Dowell Chemical Co.,Ltd | +86-0311-89805679 +8613463963265 | sell@dowechem.com | China | 56 | 58 |
2-[[(1,1-Dimethylethoxy)carbonyl]amino]-4-pyridinecarboxylic acidmethylester
Methyl 2-(Boc-amino)isonicotinate
4-Pyridinecarboxylic acid, 2-[[(1,1-diMethylethoxy)carbonyl]aMino]-, Methyl ester
Methyl 2-((tert-butoxycarbonyl)aMino)isonicotinate
2-Boc-amino-isonicotinic acid methyl ester
2-tert-Butoxycarbonylamino-isonicotinic acid methyl ester
Methyl 2-[(2-methylpropan-2-yl)oxycarbonylamino]pyridine-4-carboxylate
methyl 2-(tert-butoxycarbonylamino)pyridine-4-carboxylate
639091-75-1