Nandrolone phenylpropionate

Nandrolone phenylpropionate 구조식 이미지
카스 번호:
62-90-8
상품명:
Nandrolone phenylpropionate
동의어(영문):
NTPP;19Ntpp;Activin;Durabol;Nerobil;SK 22271;NSC-23162;Durabolin;Fenobolin;Nandrolin
CBNumber:
CB3680120
분자식:
C27H34O3
포뮬러 무게:
406.57
MOL 파일:
62-90-8.mol

Nandrolone phenylpropionate 속성

녹는점
85-87°C
알파
D +58° (chloroform)
끓는 점
487.61°C (rough estimate)
밀도
1.0140 (rough estimate)
굴절률
1.5460 (estimate)
저장 조건
Controlled Substance, -20°C Freezer
용해도
DMSO : 100 mg/mL (245.97 mM; Need ultrasonic)
물리적 상태
고체
물리적 상태
단단한 모양
색상
흰색에서 황백색까지
InChIKey
UBWXUGDQUBIEIZ-QNTYDACNSA-N
SMILES
C[C@]12CC[C@]3([H])[C@@]4([H])CCC(=O)C=C4CC[C@@]3([H])[C@]1([H])CC[C@@H]2OC(=O)CCC1C=CC=CC=1 |&1:1,4,6,16,18,22,r|
CAS 데이터베이스
62-90-8(CAS DataBase Reference)
NIST
4-Androstene-17-beta-ol-3-one, 19-nor-delta-, phenylpropionate(62-90-8)
안전
  • 위험 및 안전 성명
  • 위험 및 사전주의 사항 (GHS)
위험품 표기 Xn
위험 카페고리 넘버 20/21/22-40
안전지침서 23-36
RTECS 번호 KG7995000
독성 LD50 intraperitoneal in mouse: > 1gm/kg
그림문자(GHS): GHS hazard pictograms
신호 어: Danger
유해·위험 문구:
암호 유해·위험 문구 위험 등급 범주 신호 어 그림 문자 P- 코드
H351 암을 일으킬 것으로 의심됨 (노출되어도 암을 일으키지 않는다는 결정적인 증거가 있는 노출경로가 있다면 노출경로 기재) 발암성 물질 구분 2 경고 P201, P202, P281, P308+P313, P405,P501
예방조치문구:
P201 사용 전 취급 설명서를 확보하시오.
P308+P313 노출 또는 접촉이 우려되면 의학적인 조치· 조언를 구하시오.

Nandrolone phenylpropionate C화학적 특성, 용도, 생산

화학적 성질

White to Off-White Solid

용도

Anabolic steroid; androgen.

World Health Organization (WHO)

Nandrolone phenylpropionate, an anabolic steroid, was introduced in 1959. In 1982, low dosage preparations were prohibited in Bangladesh due to inadmissible promotion of products containing anabolic steroids for malnourished children. Higher dosage preparations of nandrolone phenylpropionate remain available in many countries, including Bangladesh, for several highly specific but limited indications that apply to patients with chronic debilitating and emaciating diseases, particularly associated with neoplasia and some types of aplastic anaemia.

Synthesis

Nandrolone phenylpropionate is prepared by reacting anhydrous MeCN with a mixture of 3-phenylpropanoic acid, aryneprecursor, nandrolone CsF, K2CO3, and 18-crown-6 in 70 ?? in an oil bath.
Add anhydrous MeCN (0.5 mL) to a mixture of 3-phenylpropanoic acid (30.0 mg, 0.2 mmol, 1.0 equiv), aryneprecursor (119.2 mg, 0.4 mmol, 2.0 equiv), nandrolone (82.3 mg, 0.3 mmol, 1.5 equiv), CsF (182.3 mg, 1.2 mmol, 6.0 equiv), K2CO3 (82.9 mg, 0.6 mmol, 3.0 equiv), and 18-crown-6 (158.6 mg, 0.6 mmol, 3.0 equiv). Warm the mixture to 70 ?? in an oil bath and stir at this temperature for8 hours. Remove all the volatiles directly on rotary evaporator. Purify by flash column chromatography with pet ether:EtOAc = 20:1. 1H NMR (400 MHz, CDCl3) |? 7.31-7.26(m,2H), 7.23-7.17(m,3H), 5.83 (s, lH), 4.65-4.58(m, lH), 2.95(t, J= 8.0 Hz,2H), 2.64(t, J= 8.0 Hz,2H), 2.51-2.36(m, 2H), 2.31-2.04(m, 5H), 1.86-1.79(m, 2H), 1.72-1.61 (m, 2H), 1.57-1.00(m, 8H),0.90-0.81(m, 1H), 0.79 (s, 3H)ppm.
Synthesis_62-90-8Fig The synthetic method 1 of Nandrolone phenylpropionate

Nandrolone phenylpropionate 준비 용품 및 원자재

원자재

준비 용품


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