BIS(2,2,2-TRIFLUOROETHYL)인산염
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BIS(2,2,2-TRIFLUOROETHYL)인산염 속성
- 끓는 점
- 43-44 °C/2 mmHg (lit.)
- 밀도
- 1.545 g/mL at 25 °C (lit.)
- 굴절률
- n
20/D 1.332(lit.)
- 인화점
- 169 °F
- 물리적 상태
- 액체
- 색상
- 무색 내지 거의 무색
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
위험품 표기 | Xi | ||
---|---|---|---|
위험 카페고리 넘버 | 36/37/38 | ||
안전지침서 | 23-26-28-36 | ||
WGK 독일 | 3 | ||
HS 번호 | 2920.90.5100 |
BIS(2,2,2-TRIFLUOROETHYL)인산염 C화학적 특성, 용도, 생산
Synthesis Reference(s)
Synthesis, p. 410, 1984 DOI: 10.1055/s-1984-30856Synthesis
The synthesis method of Bis(2,2,2-trifluoroethyl) Phosphite is as follows: A solution of phosphorus trichloride (43.5 mL, 0.50 mol) in dichloromethane (100 mL) was placed in an oven dried 1L round bottom flask. A reflux condenser and pressure equalizing addition funnel were attached to the round bottom flask. The addition funnel was charged with a solution of 2-methyl-2-propanol (48.0 mL, 0.50 mol) in dichloromethane (100 mL), and then the contents of the addition funnel were added in a dropwise manner to the round bottom flask under argon gas at 0 ℃over the course of 30 min. The reaction mixture was allowed to stir for an additional 30 min, then the addition funnel is recharged with a solution of 2,2,2-trifluoroethanol (70.0 mL, 0.96 mol) and dichloromethane (100 mL) and then the contents of the addition funnel were added in a dropwise manner to the round bottom flask under argon gas at 0 ℃ over the course of 30 min. The reaction mixture was then allowed to stir at RT overnight. The gaseous vapors were then degassed into NaOH (30.2 g, 0.98 mol) in 200 mL of water over the course of 8 hrs. The solvents were removed by rotary evaporation and the crude material was fractionally distilled under reduced pressure yielding Bis(2,2,2-trifluoroethyl) Phosphite (100.89 g, 0.41 mol, 82.2%) as colorless liquid.BIS(2,2,2-TRIFLUOROETHYL)인산염 준비 용품 및 원자재
원자재
준비 용품
BIS(2,2,2-TRIFLUOROETHYL)인산염 공급 업체
글로벌( 50)공급 업체
공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
---|---|---|---|---|---|
Hubei xin bonus chemical co. LTD | 86-13657291602 |
linda@hubeijusheng.com | CHINA | 22968 | 58 |
career henan chemical co | +86-0371-86658258 +8613203830695 |
factory@coreychem.com | China | 29826 | 58 |
Shaanxi Dideu Medichem Co. Ltd | 18192627656 |
1012@dideu.com | China | 1328 | 58 |
Career Henan Chemica Co | +86-0371-86658258 +8613203830695 |
laboratory@coreychem.com | China | 30253 | 58 |
Dayang Chem (Hangzhou) Co.,Ltd. | 571-88938639 +8617705817739 |
info@dycnchem.com | China | 52861 | 58 |
LEAP CHEM CO., LTD. | +86-852-30606658 |
market18@leapchem.com | China | 24738 | 58 |
Aladdin Scientific | +1-+1(833)-552-7181 |
sales@aladdinsci.com | United States | 57511 | 58 |
Amadis Chemical Company Limited | 571-89925085 |
sales@amadischem.com | China | 131980 | 58 |
J & K SCIENTIFIC LTD. | 010-82848833 400-666-7788 |
jkinfo@jkchemical.com | China | 96815 | 76 |
Meryer (Shanghai) Chemical Technology Co., Ltd. | 021-61259108 18621169109 |
market03@meryer.com | China | 40240 | 62 |
BIS(2,2,2-TRIFLUOROETHYL)인산염 관련 검색:
BIS(2,2,2-TRIFLUOROETHYL) (METHOXYCARBONYLMETHYL)PHOSPHONATE
Phosphite
BIS(2,2,2-TRIFLUOROETHYL) PHOSPHITE
alamifovir
[BIS-(2,2,2-TRIFLUORO-ETHOXY)-PHOSPHORYL]-BROMO-ACETIC ACID METHYL ESTER
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BIS-(2,2,2-TRIFLUOROETHYL) METHOXYCARBONYLMETHYL PHOSPHONATE, [1,2-14C]
ETHYL 2-[BIS(2,2,2-TRIFLUOROETHYL)PHOSPHONO] PROPIONATE
[2-(2-AMINO-6-CHLORO-PURIN-9-YL)-ETHOXYMETHYL]-PHOSPHONIC ACID BIS-(2,2,2-TRIFLUORO-ETHYL) ESTER
TRIS(2,2,2-TRIFLUOROETHYL)PHOSPHATE
BIS(TRIFLUOROETHYL) METHYLPHOSPHONATE