1-Boc-3-piperidone
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1-Boc-3-piperidone 속성
- 녹는점
- 35-40 °C (lit.)
- 끓는 점
- 289.8±33.0 °C(Predicted)
- 밀도
- 1.099±0.06 g/cm3(Predicted)
- 인화점
- >230 °F
- 저장 조건
- 2-8°C
- 산도 계수 (pKa)
- -1.71±0.20(Predicted)
- 물리적 상태
- 액체
- 색상
- 무색의
- 수용성
- 물에 녹지 않습니다.
- BRN
- 5936353
- InChI
- InChI=1S/C10H17NO3/c1-10(2,3)14-9(13)11-6-4-5-8(12)7-11/h4-7H2,1-3H3
- InChIKey
- RIFXIGDBUBXKEI-UHFFFAOYSA-N
- SMILES
- N1(C(OC(C)(C)C)=O)CCCC(=O)C1
- CAS 데이터베이스
- 98977-36-7(CAS DataBase Reference)
안전
- 위험 및 안전 성명
- 위험 및 사전주의 사항 (GHS)
| 안전지침서 | 24/25 | ||
|---|---|---|---|
| WGK 독일 | 3 | ||
| 위험 등급 | KEEP COLD | ||
| HS 번호 | 29339900 |
1-Boc-3-piperidone C화학적 특성, 용도, 생산
화학적 성질
White to yellow low melting solid용도
1-Boc-3-piperidone, is used as an important raw material and intermediate used in organic Synthesis, pharmaceuticals, agrochemicals and dyestuff.Synthesis
With 179g compound 3(1-BOC-3-piperidines alcohol) drop in the 2L reaction flask, drop into pimelinketone 1300g, aluminum isopropylate 88g, methylene dichloride 400ml is warming up to 80 ℃, insulation reaction 8h, reaction finishes to be cooled to room temperature, adds 10% sodium hydroxide 200ml, stirring at normal temperature 30min, filter, the filtrate normal pressure reclaims methylene dichloride, reclaim under reduced pressure pimelinketone again, reclaim finish after, add the 300ml dichloromethane extraction three times, it is dry concentrated to merge oil reservoir, gets 1-BOC-3-piperidone crude product.Refining: with 1-BOC-3-piperidone crude product is that 60pa, temperature are to distill under 104 ~ 105 ℃ the condition at pressure, gets 1-BOC-3-piperidone elaboration 163g, 92.9%.
1-Boc-3-piperidone 준비 용품 및 원자재
원자재
준비 용품
(S)-3-Amino-1-N-Boc-piperidine
3-HYDROXY-3-PHENYL-PIPERIDINE
6-METHOXY-1,2,3,4-TETRAHYDRO-BETA-CARBOLINE
4,5,6,7-tetrahydro-1-methyl-1H-Pyrazolo[3,4-c]pyridine
아세톤
tert-butyl 3-(isopropylamino)piperidine-1-carboxylate
5-(Toluene-4-sulfonyloxy)-3,4-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester
TERT-BUTYL 3-(N-BENZYL-N-METHYLAMINO) PIPERIDINE-1-CARBOXYLATE
1-N-BOC-3-HYDROXY-3-PHENYLPIPERIDINE
1-Boc-3-piperidone 공급 업체
글로벌( 499)공급 업체
| 공급자 | 전화 | 이메일 | 국가 | 제품 수 | 이점 |
|---|---|---|---|---|---|
| Chongqing Ensky Pharmaceutical Co.,Ltd. | +86-23-86815286 +86-13983794297 |
sales@ensky-chemical.com | China | 88 | 58 |
| Shanghai Quedan biology science and technology co., ltd | +86-13004146052 |
lnzc@quedan.com.cn | China | 1060 | 58 |
| Anhui Yisheng Technology Co., LTD | +86-19355901310 +86-19355901310 |
alice@ah-yisheng.com | China | 333 | 58 |
| Zhengzhou Lingzhiyue Technology Co., Ltd | +86-0371-55074660 +86-13783527580 |
Lingzhiyue@aliyun.com | China | 3144 | 58 |
| Anhui Yiao New Material Technology Co., Ltd | +86-199-55145978 +8619955145978 |
sales8@anhuiyiao.com | China | 253 | 58 |
| Xiamen Wonderful Bio Technology Co., Ltd. | +8613043004613 |
Sara@xmwonderfulbio.com | China | 305 | 58 |
| Shandong Huisheng Import & Export Co., Ltd. | +86-13176845580 +86-13176845580 |
da@zhongda-biotech.com | China | 248 | 58 |
| Anhui Zhongda Biotechnology Co., Ltd | +8619956560829 |
justine@zhongda-biotech.com | China | 300 | 58 |
| Anhui Zhongda Biotechnology Co., Ltd | +8615689548120 |
linda@zhongda-biotech.com | China | 204 | 58 |
| Anhui Ruihan Technology Co., Ltd | +8617756083858 |
daisy@anhuiruihan.com | China | 994 | 58 |