2-甲氧基吡啶(1628-89-3)核磁图(13CNMR)
InChI:InChI=1S/C6H7NO/c1-8-6-4-2-3-5-7-6/h2-5H,1H3
InChIKey: IWTFOFMTUOBLHG-UHFFFAOYSA-N
Smiles:C1(OC)=NC=CC=C1
-
Mass
MS-NW-8329
2-methoxypyridine
C6H7NO (Mass of molecular ion: 109)
Source Temperature: 260 °C
Sample Temperature: 130 °C
Reservoir, 75 eV
15.0 3.6
26.0 3.2
27.0 5.7
28.0 5.9
29.0 1.7
37.0 4.3
38.0 12.3
39.0 31.3
40.0 4.4
41.0 1.7
42.0 4.2
49.0 1.6
50.0 8.4
51.0 20.7
52.0 55.5
53.0 11.4
54.0 1.4
55.0 1.8
64.0 2.9
65.0 2.8
66.0 7.1
67.0 1.1
75.0 1.2
76.0 1.8
78.0 22.6
79.0 100.0
80.0 31.5
81.0 2.8
93.0 1.4
106.0 1.7
108.0 73.5
109.0 60.2
110.0 4.5
113.0 3.5
115.0 1.1
90 MHz in CDCl3
400 MHz in CDCl3
-
| 1H NMR |
89.56 MHz |
| C6 H7 N O
|
0.05 ml : 0.5 ml CDCl3
|
| 2-methoxypyridine
|
 |
Assign. Shift(ppm)
A 8.152
B 7.505
C 6.810
E 6.715
E 3.917
|
Hz ppm Int.
733.88 8.195 50
733.19 8.187 52
732.00 8.174 56
728.88 8.139 55
728.31 8.133 56
726.94 8.117 57
681.38 7.609 43
679.38 7.586 40
674.25 7.529 59
673.06 7.516 64
672.25 7.507 58
671.06 7.493 50
666.00 7.437 63
664.00 7.415 56
616.50 6.884 62
615.56 6.874 67
611.44 6.828 60
610.50 6.817 77
609.44 6.805 63
608.50 6.795 60
606.19 6.769 98
605.31 6.759 133
604.38 6.749 99
603.50 6.739 55
597.88 6.676 69
597.06 6.667 94
350.88 3.918 1000
-
| 1H NMR |
399.65 MHz |
| C6 H7 N O
|
0.05 ml : 0.5 ml CDCl3
|
| 2-methoxypyridine
|
|
Assign. Shift(ppm)
A 8.157
B 7.517
C 6.824
D 6.724
E 3.921
|
Hz ppm Int.
3263.92 8.167 94
3263.18 8.166 102
3261.96 8.163 105
3261.23 8.161 99
3258.91 8.155 96
3258.06 8.153 103
3256.84 8.150 102
3256.10 8.148 97
3013.06 7.540 114
3011.11 7.535 121
3006.10 7.522 128
3004.76 7.519 145
3004.03 7.517 145
3002.69 7.514 130
2997.68 7.501 132
2995.61 7.496 125
2733.64 6.841 127
2732.79 6.838 133
2728.64 6.828 131
2727.66 6.826 144
2726.56 6.823 133
2725.71 6.821 129
2721.56 6.810 121
2720.58 6.808 127
2692.14 6.737 156
2691.28 6.735 238
2690.31 6.732 152
2683.84 6.716 137
2682.86 6.714 222
2682.01 6.711 144
1567.02 3.921 1000