Iodomethyl pivalate
Iodomethyl pivalate атрибут
| Температура плавления: |
33-35 °C(lit.) |
| Температура кипения: |
211.5 °C(lit.) |
| плотность: |
1.614±0.06 g/cm3(Predicted) |
| показатель преломления: |
1.4830 to 1.4870 |
| Fp: |
194 °F |
| температура хранения: |
Refrigerator, under inert atmosphere |
| растворимость: |
Хлороформ (Слегка), Метанол (Слегка) |
| форма: |
Масло |
| цвет: |
Желтый |
| Чувствительный: |
Light, Air and Heat Sensitive |
| InChI: |
InChI=1S/C6H11IO2/c1-6(2,3)5(8)9-4-7/h4H2,1-3H3 |
| ИнЧИКей: |
PELJISAVHGXLAL-UHFFFAOYSA-N |
| SMILES: |
C(OCI)(=O)C(C)(C)C |
| Справочник по базе данных CAS: |
53064-79-2(CAS DataBase Reference) |
Iodomethyl pivalate химические свойства, назначение, производство
Химические свойства
Pale Yellow Liquid
Использование
Iodomethyl pivalate can be used as reagent used for the addition of pivaloyl group.
Ссылки на синтез
Синтез
Iodomethyl pivalate is synthesised using chloromethyl pivalate as a raw material by chemical reaction. The specific synthesis steps are as follows:
Three bottles were added 10.0 g of chloromethyl pivalate, Ethyl acetate 30 mL, 11.6 g of sodium iodide and 3.6 g of calcium chloride, After heating to 78 ° C for 6 h, Cooling to 0 ,Then washed with 5% sodium thiosulfate to colorless, Dried over anhydrous magnesium sulfate, Concentrated under reduced pressure. 16 g of a yellow liquid. Iodomethyl pivalate was obtained. The reaction molar yield was 94% and GC: 98%.
Iodomethyl pivalate препаратная продукция и сырье
сырьё
препарат
Iodomethyl pivalate поставщик
Global( 214)Suppliers
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