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Меларсопрол

Меларсопрол структура
494-79-1
CAS №
494-79-1
Химическое название:
Меларсопрол
английское имя:
melarsoprol
Синонимы:
RP3854;Arsobal;melarsoprol;Melarsoprolum;Melarsoprol (Mixture of DiastereoMers);2-[4-(4,6-Diamino-1,3,5-triazine-2-ylamino)phenyl]-1,3,2-dithiarsolane-4-methanol;[2-[4-[(4,6-diamino-s-triazin-2-yl)amino]phenyl]-1,3,2-dithiarsolan-4-yl]methanol;2-[4-[(4,6-Diamino-1,3,5-triazin-2-yl)amino]phenyl]-1,3,2-dithiarsolane-4-methanol;1,3,2-Dithiarsolane-4-methanol, 2-[4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl]-;[2-[4-[(4,6-diamino-1,3,5-triazin-2-yl)amino]phenyl]-1,3,2-dithiarsolan-4-yl]methanol
CBNumber:
CB5911778
Формула:
C12H15AsN6OS2
молекулярный вес:
398.345
MOL File:
494-79-1.mol

Меларсопрол атрибут

растворимость: DMSO (Slightly), Methanol (Slightly, Heated)
форма: Solid
цвет: White to Off-White
FDA UNII: ZF3786Q2E8
Код УВД: P01CD01
безопасность
  • Заявления о рисках и безопасности
  • код информации об опасности(GHS)
символ(GHS) GHS hazard pictogramsGHS hazard pictograms
сигнальное слово Danger
Заявление об опасности
пароль Заявление об опасности Класс опасности категория сигнальное слово пиктограмма предупреждение
H301 Токсично при проглатывании. Острая токсичность, пероральная Категория 3 Опасность GHS hazard pictograms P264, P270, P301+P310, P321, P330,P405, P501
H410 Чрезвычайно токсично для водных организмов с долгосрочными последствиями. Опасность для водной среды, долгосрочная опасность Категория 1 Предупреждение GHS hazard pictograms P273, P391, P501
H331 Токсично при вдыхании. Острая токсичность, ингаляционная Категория 3 Опасность GHS hazard pictograms P261, P271, P304+P340, P311, P321,P403+P233, P405, P501
Внимание
P261 Избегать вдыхания пыли/ дыма/ газа/ тумана/ паров/ аэрозолей.
P264 После работы тщательно вымыть кожу.
P270 При использовании продукции не курить, не пить, не принимать пищу.
P271 Использовать только на открытом воздухе или в хорошо вентилируемом помещении.
P273 Избегать попадания в окружающую среду.
P301+P310 ПРИ ПРОГЛАТЫВАНИИ: Немедленно обратиться за медицинской помощью. Прополоскать рот.
P304+P340 ПРИ ВДЫХАНИИ: Свежий воздух, покой.
P311 Обратиться за медицинской помощью.
P391 Ликвидировать просыпания/проливы/утечки.
P403+P233 Хранить в хорошо вентилируемом месте в плотно закрытой/герметичной таре.
P405 Хранить в недоступном для посторонних месте.
P501 Удалить содержимое/ контейнер на утвержденных станциях утилизации отходов.

Меларсопрол химические свойства, назначение, производство

Описание

Knowingly or unknowingly, arsenic-containing drugs have been used for treatment of parasitic conditions for thousands of years. In the late 1800s and early 1900s, Paul Ehrlich introduced the use of trivalent arsenicals. Melarsoprol, an organoarsenical, came into use in the late 1940s, and it remains the first-choice drug in the treatment of trypanosomiasis. Until 1990, it also was the only treatment for late-stage sleeping sickness.

Использование

Melarsoprol is a drug used for the treatment of African trypanosomes, a sleeping sickness in humans, a disease that is typically fatal without chemotherapy.

Антимикробная активность

It is highly and rapidly active against Trypanosoma brucei gambiense and T. brucei rhodesiense in vitro at submicromolar concentrations. It is much less active against the trypanosomes that infect domestic animals, T. congolense and T. vivax. Co-administration with eflornithine is effective against central nervous system (CNS) infection with T. brucei in rodent models, but clinical studies have found the combination less effective than nifurtimox–eflornithine.

Приобретенная устойчивость

Up to 25% of cases of T. brucei gambiense in Central Africa relapse. Patients infected with T. brucei rhodesiense normally respond to a second course of the drug, but those with T. brucei gambiense do not. In laboratory-generated resistant strains, decreased sensitivity results from reduced uptake of the drug by bloodstream trypomastigotes that either lack an adenine/adenosine transporter (TbAT1) or contain a transporter gene with point mutations. There is conflicting evidence about the role of this mechanism of resistance in isolates from patients unresponsive to treatment.

Угроза здоровью

Melarsoprol (4, Mel B, Arsobal C12H15AsN6OS2) is applied for T. b. gambiense or T. b. rhodesiense. The drug, administered intravenously, is a solution containing a combination of BAL (2,3-dimercaptopropanol) and the trivalent arsenic compound, melarsen oxide. Not only can the drug cause serious side effects such as intense dermal irritation, myocarditis, and renal and hepatic damage, but it is also responsible for death in 5% of patients.

Фармацевтические приложения

Mel B. A derivative of trivalent melarsen oxide and dimercaprol (BAL), possessing a melaminyl moiety. Formulated in 3.6% propylene glycol for intravenous administration. It is almost insoluble in water.

Механизм действия

It generally is accepted that the enzyme with which melarsoprol reacts is an enzyme involved in glycolysis, and as a result, inhibition of pyruvate kinase occurs. It is argued, however, that the inhibition may not occur at pyruvate kinase but, rather, at a step before the pyruvate kinase. Blockage of glycolysis would be expected to lead to loss of motility and cell lysis. More recently, Fairlamb et al. have proposed a mechanism of action that results in the inhibition of trypanothione reductase through the formation of a stable complex between melaroprol and trypanothione. Melarsoprol reacts with the cysteine sulfhydryl of trypanothione to form the stable adduct shown in Figure 39.10. Supportive of this mechanism is the synergistic action of melarsoprol with eflornithine (DMFO). Two drugs that produce sequential blockage of the synthesis of trypanothione.

Фармакокине?тика

Serum levels of 2–4 mg/L were achieved 24 h after administration of 3.6 mg/kg, falling to 0.1 mg/L at 120 h after the fourth daily injection. Elimination was biphasic with a half-life of 35 h. The volume of distribution was 100 L. It is rapidly metabolized by microsomal enzymes to melarsen oxide, reaching maximum plasma concentration by 15 min and eliminated with a half-life of 3.9 h. This metabolite can cross the blood–brain barrier and effect a CNS cure in mice. Levels of melarsoprol in the cerebrospinal fluid (CSF) reached around 300 μg/L, about 50 times lower than serum levels.

Клиническое использование

2-p-(4,6-Diamino-s-triazin-2-yl-amino)phenyl-4-hydroxymethyl-1,3,2-dithiarsoline (Mel B, Arsobal) is prepared byreduction of a corresponding pentavalent arsanilate to thetrivalent arsenoxide followed by reaction of the latter with2,3-dimercapto-1-propanol (British anti-Lewisite [BAL]). Ithas become the drug of choice for the treatment of thelater stages of both forms of African trypanosomiasis.Melarsoprol has the advantage of excellent penetration intothe CNS and, therefore, is effective against meningoencephaliticforms of T. gambiense and T. rhodesiense.Trivalent arsenicals tend to be more toxic to the host (as wellas the parasites) than the corresponding pentavalent compounds.The bonding of arsenic with sulfur atoms tends toreduce host toxicity, increase chemical stability (to oxidation),and improve distribution of the compound to the arsenoxide.Melarsoprol shares the toxic properties of other arsenicals, however, so its use must be monitored for signsof arsenic toxicity.

Побочные эффекты

The propylene glycol formulation can cause tissue trauma and long-term damage to veins. Drug-induced reactions include fever on first administration, abdominal colic pain, dermatitis and arthralgia. Polyneuropathy has been reported in about 10% of patients. Reactive arsenical encephalopathy is a serious side effect that occurs in around 10% of those treated, with death in 1–3% of cases. The frequency of encephalopathy increases with a rise in the white cell count or the presence of trypanosomes in the CSF. The causes of the immunological responses involved in the encephalopathy and the possible existence of two forms (reactive and hemorrhagic) are not completely resolved. Studies to identify antiinflammatory approaches to reduce reactive encephalopathy in late-stage T. brucei gambiense infection have produced limited results.

Метаболизм

Melarsoprol is administered IV in multiple doses and multiple sessions. Its major metabolite in humans is the lipophilic melarsen oxide, which can penetrate into the CNS. This metabolite apparently is responsible for the protein-binding characteristic for melarsoprol.

Меларсопрол препаратная продукция и сырье

сырьё

препарат


Меларсопрол поставщик

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