1-(1-Propenyl)-4-methylbenzene synthesis
- Product Name:1-(1-Propenyl)-4-methylbenzene
- CAS Number:2698-14-8
- Molecular formula:C10H12
- Molecular Weight:132.2
Yield:2698-14-8 90%
Reaction Conditions:
Stage #1: ethyltriphenylphosphonium bromidewith n-butyllithium in tetrahydrofuran at 0; for 0.5 h;Inert atmosphere;
Stage #2: 4-methyl-benzaldehyde in tetrahydrofuran at 0 - 50; for 12 h;Inert atmosphere;
References:
Jiang, Xiaomin;Lan, Guangxu;Lin, Wenbin;Ni, Kaiyuan;Quan, Yangjian;Shi, Wenjie;Song, Yang;Wang, Cheng [Journal of the American Chemical Society,2021,vol. 143,# 40,p. 16718 - 16724] Location in patent:supporting information
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