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ChemicalBook CAS DataBase List 1,3-BIS(2,6-DI-I-PROPYLPHENYL)IMIDAZOL-2-YLIDENE
244187-81-3

1,3-BIS(2,6-DI-I-PROPYLPHENYL)IMIDAZOL-2-YLIDENE synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 77.5 percent / formic acid / ethanol; H2O / 48 h
2.1: toluene / 100 °C
2.2: 47 percent / HCl / toluene; dioxane / 5 h / 70 °C
3.1: 79 percent / KOt-Bu / tetrahydrofuran / 4 h / 20 °C

References:

Jafarpour, Laleh;Stevens, Edwin D.;Nolan, Steven P. [Journal of Organometallic Chemistry,2000,vol. 606,# 1,p. 49 - 54]

FullText

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