Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 1,4-Cyclohexanedione
637-88-7

1,4-Cyclohexanedione synthesis

13synthesis methods
2,5-Dicarbethoxy-1,4-cyclohexanedione has been prepared by the self-condensation of diethyl succinate by use of sodium or sodium ethoxide catalyst (with or without a solvent) and by reaction of ethyl 4-bromo-3-ketobutanoate or ethyl 4-chloro-3-ketobutanoate with sodium ethoxide in ethanol.
1,4-Cyclohexanedione has been prepared by hydrolysis and decarboxylation of 2,5-dicarbethoxy-1,4-cyclohexanedione by using concentrated sulfuric acid, aqueous alcoholic phosphoric acid, or water at 195–200°, and by peroxyvanadic acid oxidation of cyclohexanone.
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: water / 48 h / 20 °C / 750.08 Torr / Electrolysis
2: water / 48 h / 20 °C / 750.08 Torr / Electrolysis

References:

Bugnola, Marco;Shen, Kaiji;Haviv, Eynat;Neumann, Ronny [ACS Catalysis,2020,vol. 10,# 7,p. 4227 - 4237]

1,4-Cyclohexanedione Related Search: