1,4-DiMethoxybenzene-D6 synthesis
2synthesis methods
- Product Name:1,4-DiMethoxybenzene-D6
- CAS Number:24658-26-2
- Molecular formula:C8H4D6O2
- Molecular Weight:144.2008
Yield:24658-26-2 98%
Reaction Conditions:
Stage #1: hydroquinonewith potassium hydroxide;tetrabutylammomium bromide at 20;
Stage #2: iodomethane-d3 at 40 - 45; for 72 h;Further stages.;
References:
Xu, Ya-Zhu;Lin, Huei-Ru;Lua, Chang-Ahai;Chen, Chinpiao [Journal of the Chinese Chemical Society,2007,vol. 54,# 2,p. 493 - 502]
