1 5-DICHLORO-3-PENTANONE synthesis
- Product Name:1 5-DICHLORO-3-PENTANONE
- CAS Number:3592-25-4
- Molecular formula:C5H8Cl2O
- Molecular Weight:155.02
74-85-1
96 suppliers
$79.00/11l
625-36-5
359 suppliers
$45.00/100ml
3592-25-4
120 suppliers
$20.00/100mg
Yield:3592-25-4 95%
Reaction Conditions:
with aluminum (III) chloride
Steps:
3.1
The 1,5-diaminopentan-3-ol 6 was synthesized in 4 stages from ethylene and 3-chloropropionyl chloride with an overall yield of 54% according to a reaction scheme described in the references below: Bull. Chem. Soc. Jpn., 55: 2404-2408 (1982); Bull. Chem. Soc. Jpn., 65: 334-339 (1992); Bull. Chem. Soc. Jpn., 75: 2595-2607 (2002); Recl. Trav. Chim. Pays-Bas, 112: 535-548 (1993); J. Chem. Soc. (C) Organic 17: 2401-2403 (1976); and European Patent Application No. 0 872 466 A1
References:
Sabelle, Stéphane;Metais, Eric;Bordier, Thierry US2007/11827, 2007, A1 Location in patent:Page/Page column 9
625-36-5
359 suppliers
$45.00/100ml
3592-25-4
120 suppliers
$20.00/100mg
74-85-1
96 suppliers
$79.00/11l
625-36-5
359 suppliers
$45.00/100ml
7429-90-5
8 suppliers
$9.00/5g
3592-25-4
120 suppliers
$20.00/100mg